研究目的
Investigating the effects of powder reuse on powder size distribution, morphology, and chemistry during selective laser melting (SLM) additive manufacturing of 316 stainless steel, with a focus on oxygen pickup mechanisms.
研究成果
The research concluded that oxygen content in unmelted 316L powder varies as a function of its position relative to the heat source during SLM, with significant oxygen pickup observed near melt zones. The volume of melted material did not correlate well with oxygen pickup. The study highlighted the importance of understanding localized oxidation in powder bed additive manufacturing for future recyclability studies.
研究不足
The study was limited by the inability to measure oxide layer growth directly due to the impracticality of finding a particle that resided close to the melted region and experienced enhanced oxide growth. Additionally, the DICTRA model overestimated oxide thickness due to simplifications in the thermal history calculations.
1:Experimental Design and Method Selection:
The study focused on identifying and describing local powder bed degradation during the SLM process using a Renishaw AM250 instrument.
2:Sample Selection and Data Sources:
Virgin stainless steel 316L powder was used as feedstock, and samples were collected from various channel widths post-process for analysis.
3:List of Experimental Equipment and Materials:
Equipment included a Renishaw AM250 instrument, Bruker D2Phaser desktop diffractometer, Horiba La950 V2 Laser Diffraction Particle Analyzer, and X-ray photoelectron spectroscopy (XPS) at ORNL’s MST Division.
4:Experimental Procedures and Operational Workflow:
The build chamber was evacuated and refilled with argon cover gas, and powder samples were collected from channels post-process for analysis.
5:Data Analysis Methods:
Data were analyzed using X-ray diffraction for phase analysis, laser diffraction for size distribution, bulk chemical analysis for oxygen content, and XPS for surface composition.
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