研究目的
To evaluate the role and effectiveness of using a graphite layer as an absorbing coating during pulsed laser impact on the surface of Y–TZP ceramics to produce technological recommendations for the modification of the defective layer.
研究成果
The graphite layer significantly increases the fraction of absorbed laser radiation, leading to heating, melting, and evaporation of Y–TZP ceramics under less intense modes. This modification favorably affects the use of pulsed laser radiation for surface modification, allowing for more efficient treatment of ceramic parts with large working areas.
研究不足
The study focuses on the effect of a graphite layer on the surface of Y–TZP ceramics under pulsed laser irradiation, but does not explore the long-term durability or performance of the modified surfaces under operational conditions. Additionally, the study is limited to specific laser parameters and does not cover a broader range of potential applications or materials.
1:5 mm/stroke, depth of grinding t = 03 mm. The graphitized surface of Y–TZP ceramics was understood as a graphite layer applied by spraying Graphit 33 aerosol composition onto the surface of samples. After applying the graphite layer, the samples changed color from white to matte graphite black (corresponding to RAL 9011). After laser treatment, residues of the graphite layer were removed with PL301 detergent; after that, the samples were washed in an ultrasonic Powersonic device. On the surface of the samples, 4 × 4 mm areas were treated using a pulsed laser U-The parameters of the pulsed laser treatment regime are as follows:
15. The parameters of the pulsed laser treatment regime are as follows: laser pulse power P 1 – 15 W, relative raster scanning speed v 25 – 200%, step size of the movement of the laser beam along the x (sx) and y (sy) axes sx = sy 10 – 60 μm. The pulse repetition rate f (30 kHz), the number of pulses in the bundle np (1 pulse) and the number of passes in a treatment cycle N (1 pass) in the experiments did not change. The diameter of the spot from the laser beam on the treated surface was 40 μm. The surface roughness Ra of the treated areas was measured along two axes (x and y) using a Hommelwerke profilograph with a TKU 300/600 probe with a sensitivity of 40 nm. The surface morphology was studied using the MikroCAD premium instrument (building a 3D model of the surface), an Olympus BX51M optical microscope and a Tescan Vega 3LMH scanning electron microscope. The adhesion strength of a graphite layer with Y–TZP ceramics was determined using a PMT-3 microhardness tester.
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Olympus BX51M optical microscope
BX51M
Olympus
Used to study the surface morphology.
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OSH-440 machine
Used for grinding the surfaces of Y–TZP ceramics samples.
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1A1B2-01 100% AC6 160/125 diamond wheel
1A1B2-01 100% AC6 160/125
Used for grinding the surfaces of Y–TZP ceramics samples.
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Graphit 33 aerosol composition
Graphit 33
Applied by spraying to create a graphite layer on the surface of Y–TZP ceramics samples.
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PL301 detergent
PL301
Used to remove residues of the graphite layer after laser treatment.
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Powersonic device
Powersonic
Used for ultrasonic washing of the samples after removing the graphite layer.
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pulsed laser U-15
U-15
Used for pulsed laser treatment of the samples.
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Hommelwerke profilograph
TKU 300/600
Hommelwerke
Used to measure the surface roughness Ra of the treated areas.
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MikroCAD premium instrument
MikroCAD premium
Used for building a 3D model of the surface.
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Tescan Vega 3LMH scanning electron microscope
Vega 3LMH
Tescan
Used to study the surface morphology.
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PMT-3 microhardness tester
PMT-3
Used to determine the adhesion strength of a graphite layer with Y–TZP ceramics.
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