研究目的
To characterise the changes suffered by the 17-4PH stainless steel powder in different grades of recycling to determine the appropriate number of reuse cycles to ensure an optimal performance of the SLM process.
研究成果
The study demonstrated morphological, chemical, and microstructural changes in SLM 17-4PH powder related to powder reuse. It is recommended to control the maximum number of powder reuse cycles and to use finer mesh sieves due to the clear relationship between the particle size and the oxides present in them.
研究不足
The study is limited to 17-4PH stainless steel powder and may not be applicable to other materials. The effects of more than 20 recycling cycles were not investigated. The study also did not explore the mechanical properties of parts manufactured from recycled powder.
1:Experimental Design and Method Selection:
The study involved morphological, chemical, and microstructural characterization of 17-4PH stainless steel powder in its original state and after 10 and 20 manufacturing reuses. The recycling process consisted of vacuuming the powder, sieving, and reloading it in the machine powder store.
2:Sample Selection and Data Sources:
The powder was classified into three states: P0 (virgin powder), P10 (10 times recycled powder), and P20 (20 times recycled powder).
3:List of Experimental Equipment and Materials:
Equipment used included a JEOL 6100 Scanning Electron Microscope (SEM), Leica KL 1500 LED plus microscope, LECO analyser, and Bruker D8 Discover diffractometer.
4:Experimental Procedures and Operational Workflow:
Morphological analysis was carried out using SEM images, chemical composition was analyzed using EDS and IGFT techniques, and microstructural analysis was performed using XRD.
5:Data Analysis Methods:
Data was analyzed using ImageJ software for morphological analysis, AZtec analysis software for EDS, and ASTM standard procedures for XRD analysis.
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