研究目的
To evaluate and characterize the interface between the graphene ?ber and matrix in graphene ?ber-reinforced composites.
研究成果
The study successfully fabricated high-performance graphene ?bers and developed a novel fragmentation test to evaluate their interfacial properties with epoxy resin. The graphene ?ber-reinforced composites exhibited superior interfacial shear stress, attributed to the physical interlocking from surface wrinkles and grooves. This work paves the way for advanced graphene ?ber-reinforced composites.
研究不足
The study focuses on the interfacial properties of graphene ?ber composites, with potential areas for optimization in the fabrication process and further exploration of the stress transfer mechanisms.
1:Experimental Design and Method Selection
Fabrication of high-strength graphene ?bers through wet spinning and thermal annealing method, and development of a novel fragmentation test to evaluate interfacial performance.
2:Sample Selection and Data Sources
Large graphene oxide (LGO) as spinning dope, graphene ?bers fabricated and reinforced single-?ber composite made.
3:List of Experimental Equipment and Materials
K2S2O8, P2O5, H3PO4, HI, KMnO4, H2O2, CaCl2, H2SO4, HCl, flake graphite, JA-02 epoxy resin.
4:Experimental Procedures and Operational Workflow
Synthesis of LGO, fabrication of graphene ?bers and composites, characterization of mechanical and interfacial properties.
5:Data Analysis Methods
Weibull distribution model for tensile strength, calculation of interfacial shear stress (IFSS) based on fragmentation test.
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