研究目的
To demonstrate a facile and low-cost technique to synthesize graphene oxide and reduced graphene oxide from battery graphite using an electrochemical method.
研究成果
The study successfully demonstrated a low-cost and environmentally benign method for synthesizing graphene oxide and reduced graphene oxide using electrochemical exfoliation of battery electrodes. The method showed promising results in terms of reducing oxygen content and maintaining electrical conductivity.
研究不足
The technique may require optimization for large-scale production and uniformity of graphene oxide and reduced graphene oxide flakes.
1:Experimental Design and Method Selection:
Electrochemical exfoliation of battery electrodes for the synthesis of graphene oxide (GO) and reduced graphene oxide (RGO) using ascorbic acid as a reducing agent.
2:Sample Selection and Data Sources:
Graphite electrodes from local batteries were used.
3:List of Experimental Equipment and Materials:
Potassium hydroxide (KOH), Sodium hydroxide (NaOH), Hydrogen peroxide (H2O2), Ammonium sulfate ((NH4)2SO4), Ascorbic acid (AA), and a regulated DC power supply.
4:Experimental Procedures and Operational Workflow:
Graphite electrodes were expanded using acid, followed by electrochemical exfoliation in an electrolyte solution. The GO was then reduced to RGO using ascorbic acid.
5:Data Analysis Methods:
Optical microscopy, UV-Vis spectroscopy, X-ray diffraction (XRD), and electrical conductivity measurements were used for characterization.
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