研究目的
Investigating the high-frequency absorption properties of gallium weakly doped barium hexaferrites for potential applications in electromagnetic compatibility and microwave absorption.
研究成果
The study demonstrates that gallium doping in barium hexaferrites affects their crystal structure, magnetic properties, and microwave absorption characteristics. The frequency of natural ferromagnetic resonance can be tuned by adjusting the Ga3+ concentration, making these materials promising for high-frequency electromagnetic radiation absorption applications.
研究不足
The study is limited to gallium weakly doped barium hexaferrites with x < 1.2. The effects of higher doping concentrations and other dopants are not explored.
1:Experimental Design and Method Selection:
The BaFe12-xGaxO19 (x <
2:2) hexaferrites were synthesised by usual ceramics technology with Bi2O3 additive. The crystal structure and unit cell parameters were refined using powder X-ray diffraction. Sample Selection and Data Sources:
Polycrystalline samples were prepared from Fe2O3, Ga2O3 oxides, and BaCO3 carbonate.
3:List of Experimental Equipment and Materials:
Powder D8 Advance diffractometer (Bruker), universal cryogenic high-field measuring system (Cryogenic Ltd), P2-68 chains scalar analyser.
4:Experimental Procedures and Operational Workflow:
Samples were sintered at 1300°C for 6 hours, cooled slowly, and their magnetic properties were investigated. Microwave properties were measured in the range of 36–56 GHz.
5:Data Analysis Methods:
X-ray diffraction data refinement was carried out by the Ritveld full-profile analysis using the FullProf program.
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