研究目的
Investigating the enhanced visible-light-driven photocatalysis of TiO2-x nanobelts/g-C3N4 nanosheets/CdS quantum dots hierarchical structure.
研究成果
The TiO2-x nanobelts/g-C3N4 nanosheets/CdS QDs ternary heterojunctions show excellent visible-light-driven photocatalytic activity, attributed to the synergistic effect of TiO2-x, g-C3N4, and CdS QDs. This study provides a promising approach for enhancing photocatalytic performance in environmental and energy applications.
研究不足
The study focuses on the photocatalytic performance under visible light irradiation and does not explore other light conditions or the long-term stability of the materials.
1:Experimental Design and Method Selection:
The ternary heterojunctions were fabricated through thermal polymerization-chemical bath deposition combined with in-situ solid-state chemical reduction approach.
2:Sample Selection and Data Sources:
TiO2 nanobelts, g-C3N4 nanosheets, and CdS quantum dots were used.
3:List of Experimental Equipment and Materials:
X-ray diffraction, Fourier transform infrared spectra, scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption, and X-ray photoelectron spectroscopy were used for characterization.
4:Experimental Procedures and Operational Workflow:
The materials were characterized and their photocatalytic activities were evaluated under visible light irradiation.
5:Data Analysis Methods:
The photocatalytic degradation ratio of Bisphenol A and hydrogen production rate were measured.
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X-ray diffractometer
D8 Advance
Bruker
Analyzing the crystal structure and phase purity of the prepared samples.
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Fourier transform infrared spectra
PerkinElmer spectrum one system
PerkinElmer
Collecting the FT-IR spectra of the samples.
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Transmission electron microscope
JEOL JEM-2010
JEOL
Recording the electron micrographs of the samples.
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UV-vis diffuse reflection spectra
UV-2550
Shimadzu
Recording the DRS spectra of the samples.
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TOC analyser
TOC-VCPN
SHIMADZU
Analyzing the total organic carbon.
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Scanning electron microscopy
Philips XL-30-ESEM-FEG
Philips
Obtaining SEM images of the samples.
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X-ray photoelectron spectroscopy
PHI-5700 ESCA
Physical Electronics
Measuring the XPS spectra of the samples.
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Electrochemical analyser
CHI660E
Shanghai
Performing electrochemical impedance spectroscopy and Mott-Schottky curve.
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Gas chromatograph
SP7800
Beijing Keruida Limited
Analyzing the photocatalytic H2 evolution.
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