研究目的
Investigating the effects of ZnO doping on the structural, dielectric, and impedance properties of Sr(Fe0.5Nb0.5)O3 ceramics.
研究成果
ZnO doped SrFe0.5Nb0.5O3 ceramics exhibited pure perovskite structures with orthorhombic symmetry. The addition of ZnO resulted in a decrease in grain size and an increase in dielectric constants, linked with Maxwell-Wagner polarization due to heterogeneous conduction in the ceramics.
研究不足
The study focuses on the effects of ZnO doping on SrFe0.5Nb0.5O3 ceramics, with specific concentrations of ZnO. The research does not explore the effects of other dopants or varying concentrations beyond 3 vol%.
1:Experimental Design and Method Selection:
The study employed a conventional mixed oxide technique for synthesizing ZnO doped SrFe0.5Nb0.5O3 ceramics. The phase formation was identified using X-ray diffraction (XRD), and microstructures were examined using a scanning electron microscope (SEM). Dielectric properties were measured using an LCR meter.
2:5Nb5O3 ceramics. The phase formation was identified using X-ray diffraction (XRD), and microstructures were examined using a scanning electron microscope (SEM). Dielectric properties were measured using an LCR meter.
Sample Selection and Data Sources:
2. Sample Selection and Data Sources: High purity powders of SrCO3, Fe2O3, and Nb2O5 were used with stoichiometric ratio. Zinc oxide (ZnO) was added with concentrations of 3 vol%.
3:List of Experimental Equipment and Materials:
X-ray diffraction (XRD), scanning electron microscope (SEM), LCR meter, high purity powders of SrCO3, Fe2O3, Nb2O5, and ZnO.
4:Experimental Procedures and Operational Workflow:
The powders were ball milled, dried, calcined, pressed into disc-shape pellets, and sintered. The sintered samples were polished, and silver paste electrodes were applied for electrical measurement.
5:Data Analysis Methods:
The dielectric properties were analyzed, and impedance spectroscopy was used to investigate the dielectric behavior linked with Maxwell-Wagner polarization.
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