研究目的
To develop and evaluate an inkjet-printed interdigital sensor for monitoring the curing process and detecting damage in nanomodified adhesively-bonded composite joints.
研究成果
The inkjet-printed interdigital sensor effectively monitored the curing process and detected damage in adhesively-bonded composite joints with minimal impact on mechanical strength. Impedance spectroscopy, enhanced by MWCNT modification, provided sensitive metrics for quality assessment and structural health monitoring, validated by thermography and SEM analysis.
研究不足
The study is limited to specific composite materials and adhesive systems; results may not generalize to other materials. The sensor's effectiveness might be affected by environmental conditions not fully explored. The artificial defect (Kapton film) may not represent all real-world defects. Optimization of sensor design for different bondline geometries was not extensively tested.
1:Experimental Design and Method Selection:
The study involved designing an interdigital capacitive sensor for impedance spectroscopy to monitor curing and damage in composite joints. The sensor was inkjet-printed directly onto the bondline, and impedance measurements were used to assess dielectric properties.
2:Sample Selection and Data Sources:
Carbon Fiber Reinforced Polymer (CFRP) single lap joints were manufactured according to ASTM D5868-01. Specimens included those with and without printed sensors, and some had artificial defects (e.g., Kapton film) for comparison.
3:Specimens included those with and without printed sensors, and some had artificial defects (e.g., Kapton film) for comparison. List of Experimental Equipment and Materials:
3. List of Experimental Equipment and Materials: Equipment included a Dimatix DMP 2850 inkjet printer, E4990A impedance analyzer, Instron universal testing machine, FLIR A615/25 IR camera, JEOL JSM 6510LV SEM, ultrasonic mixer, and laboratory oven. Materials included silver nanoparticle ink, MWCNTs (Graphistrength by Arkema), epoxy adhesive (Araldite LY 5052/Aradur 5052), and CFRP prepreg (Hexply 914-TS-5-134).
4:4). Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: Sensors were printed and sintered onto bondlines. Curing was monitored via impedance spectroscopy. Mechanical step-loading tests were conducted, with impedance and thermography measurements taken at each load step. Fracture surfaces were analyzed using SEM.
5:Data Analysis Methods:
Impedance data (e.g., Z''max, |Z|) were analyzed to correlate with curing stages and damage. Statistical analysis of mechanical strength was performed, and thermography images were processed using FFT for phase analysis.
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IR camera
A615/25
FLIR
Used for transient infrared thermography to validate damage detection.
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scanning electron microscope
JSM 6510LV
JEOL
Used to study fracture surfaces and dispersion of MWCNTs.
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inkjet printer
DMP 2850
Dimatix
Used to print the interdigital sensor electrodes onto the composite bondline.
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impedance analyzer
E4990A
Used for impedance spectroscopy measurements to monitor curing and damage.
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universal testing machine
Instron
Used for mechanical lap-shear tests to apply tensile loading.
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silver nanoparticle suspension
Sigma-Aldrich
Used as ink for printing the sensor electrodes.
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MWCNTs
Graphistrength
ARKEMA
Used to modify the epoxy adhesive for enhanced electrical properties.
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epoxy adhesive
Araldite LY 5052/Aradur 5052
Used as the adhesive for bonding the composite joints.
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CFRP prepreg
Hexply 914-TS-5-134
Used to manufacture the composite specimens.
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ultrasonic mixer
Used to disperse MWCNTs in the epoxy resin.
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laboratory oven
Used for sintering printed electrodes and curing adhesive.
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