研究目的
To develop low-cost, tunable sensing range strain sensors based on Ag nanodendrite conductive inks for wearable electronics, addressing challenges in mass production and performance.
研究成果
The Ag ND-based printed strain sensors demonstrate high performance with tunable sensing ranges and sensitivities, achieved through a low-cost, mass-producible screen-printing method. They are effective for human motion monitoring and gesture recognition, showing potential for wearable electronics and human-machine interaction applications. Future work could focus on improving hysteresis and long-term stability.
研究不足
The sensors exhibit hysteresis due to the Mullins effect of nitrile rubber and gradual aging during cyclic tests. Adhesive force between substrate and sensing layer is limited, affecting long-term stability. The production process may require optimization for higher durability and reduced hysteresis.
1:Experimental Design and Method Selection:
The study uses a one-step displacement reaction to synthesize Ag nanodendrites (NDs), formulates conductive ink with SIS binder and Disponer 904S dispersant, and employs screen printing for fabrication. The methodology includes thixotropy and contact angle tests to assess printability, and various characterizations to evaluate sensor performance.
2:Sample Selection and Data Sources:
Materials include copper foil, AgNO3, PVP, xylenes, ethanol, HCl, SIS, and Disponer 904S. Nitrile rubber is used as the substrate after cleaning. Data are collected from SEM, TEM, XRD, rheometer, contact angle meter, resistance tester, and stretching tests.
3:4S. Nitrile rubber is used as the substrate after cleaning. Data are collected from SEM, TEM, XRD, rheometer, contact angle meter, resistance tester, and stretching tests. List of Experimental Equipment and Materials:
3. List of Experimental Equipment and Materials: Equipment includes SEM (Hitachi S-4800), TEM (FEI Tecnai G2 F30), XRD (PANalytical X’Pert Pro), four-probe resistance tester (FP-001), rheometer (Kinexus Pro+), contact angle meter (SL200B/A201S), DC power supply (KXN 3002D), motorized linear stage with DY-IS controller, and Keithley-2400 multimeter. Materials are as specified in section 2.
4:Experimental Procedures and Operational Workflow:
1. 4. Experimental Procedures and Operational Workflow: Ag NDs are synthesized by immersing copper foil in AgNO3 and PVP solution, then centrifuged and washed. Conductive ink is prepared by mixing dried Ag NDs with SIS solution and Disponer 904S. Patterns are screen-printed onto substrates and dried. PSSs are fabricated by printing Ag ND ink and overprinting SIS ink, followed by drying and applying copper tape.
5:4S. Patterns are screen-printed onto substrates and dried. PSSs are fabricated by printing Ag ND ink and overprinting SIS ink, followed by drying and applying copper tape. Data Analysis Methods:
5. Data Analysis Methods: Data are analyzed using resistance measurements, SEM imaging for morphology, and statistical evaluation of sensor performance metrics like gauge factor and response time.
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SEM
S-4800
Hitachi
Observing the morphology of Ag NDs and printed layers
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TEM
Tecnai G2 F30
FEI
Transmission electron microscopy for detailed imaging of Ag NDs
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XRD
X’Pert Pro
PANalytical
Characterizing the crystal structure of Ag NDs
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Rheometer
Kinexus Pro+
Malvern Instruments
Probing thixotropic behavior of conductive ink
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Digital multimeter
Keithley-2400
Keithley
Monitoring resistance changes during tests
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Four-probe resistance tester
FP-001
Not specified
Measuring sheet resistance of conductive patterns
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Contact angle meter
SL200B/A201S
Not specified
Recording contact angle of ink on substrates
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DC power supply
KXN 3002D
ZHAOXIN
Providing power to conductive patterns
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Motorized linear stage
Not specified
Not specified
Performing stretching tests
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