研究目的
Improving the wear resistance of titanium alloys through laser cladding of composite coatings with WC reinforcement and Y2O3 addition.
研究成果
The composite coatings exhibit good metallurgical bonding, enhanced microhardness (3 times that of substrate), and improved wear resistance (7.5 times that of substrate) due to hard phases and microstructural features. Future research should focus on formation mechanisms of twins and dislocations.
研究不足
The study does not address long-term performance or environmental factors. Potential optimizations include varying laser parameters or exploring other rare earth oxides.
1:Experimental Design and Method Selection:
Laser cladding was used to deposit composite coatings on Ti-6Al-4V substrate. The study involved analyzing phases, microstructure, microhardness, and wear resistance using various techniques.
2:Sample Selection and Data Sources:
Ti6Al4V titanium alloy plates (60 mm × 40 mm × 14 mm) were used as substrates. Powder mixture of NiCrBSi, WC, and Y2O3 in weight ratio 78:20:2 was preplaced on the substrate.
3:List of Experimental Equipment and Materials:
Equipment included a fibre laser cladding system (IPG YLS-6000 fibre laser), SEM (FlexSEM 1000), TEM (Tecnai F30), XRD (Shimadzu XRD-7000), microhardness tester (HM-800), wear tester (M-200 block-on-ring, MRH-3W), and balance (TG328B). Materials included Ti-6Al-4V, NiCrBSi powder, WC powder, Y2O3 powder, SiC grit paper, acetone, organic binder, aqua regia (HCl and HNO3), and argon gas.
4:Experimental Procedures and Operational Workflow:
Substrate preparation (abrading and cleaning), powder mixing and preplacement, drying, laser cladding with specific parameters (laser power 1500 W, scanning speed 240 mm/min, gas flow 15 L/min), specimen preparation (cutting, grinding, polishing, etching), microstructure analysis (SEM, TEM, EDS, XRD), microhardness testing, and wear testing.
5:Data Analysis Methods:
XRD for phase identification, SEM and TEM for microstructure observation, EDS for element distribution, microhardness measurements, wear mass loss calculation, and statistical analysis of results.
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fibre laser
YLS-6000
IPG
Used for laser cladding process to deposit composite coatings.
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X-ray diffractometer
XRD-7000
Shimadzu
Used for phase identification of the composite coatings.
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scanning electron microscope
FlexSEM 1000
Used to investigate the microstructure of the coatings.
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transmission electron microscope
Tecnai F30
Used for detailed microstructure identification and phase analysis.
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Vickers hardness tester
HM-800
Used to measure the microhardness of the composite coatings.
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wear test machine
M-200
MRH-3W
Used to test the wear resistance of the composite coatings.
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balance
TG328B
Used to weigh the weight loss of samples after wear tests.
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