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Fabrication of Laser Grade Yb: Y2O3 Transparent Ceramics with ZrO2 Additive through Hot Isostatic Pressing
摘要： Laser grade 8 at.% Yb: Y2O3 transparent ceramics were fabricated with ZrO2 as a sintering additive by using hot isostatic pressing. The hot isostatic pressed 8 at.% Yb: Y2O3 transparent ceramics have a small average grain size of 3 μm and a high transmittance of 82.8% in the near-infrared light region. Optical homogeneity is compromised slightly in the visible light region likely because of the presence of nano/micro-scaled pores. Laser output at 1076 nm reaches a maximum power of 1.1 W and a slope efficiency of 6.1%, indicating that the hot isostatic pressed 8 at.% Yb: Y2O3 transparent ceramics have a promising optical quality. An unusual laser damage is observed and believed to be related to ZrO2 additive associated defects.
关键词： ZrO2 additive,hot isostatic pressing,laser grade,Yb: Y2O3,transparent ceramics
更新于2025-09-23 15:21:01
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[The Minerals, Metals & Materials Series] TMS 2020 149th Annual Meeting & Exhibition Supplemental Proceedings || Critical Quenching Rates After Solution Annealing: Peculiarities of Aluminuma??Silicon Alloys Fabricated by Laser Powder-Bed Fusion
摘要： Hot isostatic pressing is commonly used to reduce the porosity of (sand-)cast age-hardenable Al-alloys in order to meet the high quality requirements defined by aircraft and automotive industries. In order to establish additive manufacturing methods, such as laser powder-bed fusion (L-PBF), hot isostatic pressing can be utilized to reduce the anisotropic mechanical properties in as-built condition and at the same time eliminate porosity. For the cast aluminum alloy A356, a gas pressure of 75 MPa during hot isostatic pressing lowers the critical cooling rate required to achieve an oversaturated solid solution to about 1 K/s, which is significantly lower than the required quenching rate at atmospheric pressure (2–4 K/s). Thus, an oversaturated state of dissolved magnesium and silicon atoms within the aluminum matrix of cast alloys can easily be achieved in modern hot isostatic presses, thereby avoiding the necessity of a separate solution annealing step. In this work, we applied hot isostatic pressing followed by rapid quenching and direct aging to age-hardenable aluminum alloys processed by both sand casting and laser powder-bed fusion. It was shown that the proposed process of direct aging could be utilized for post-heat treatment of additively manufactured age-hardenable aluminum alloys to open up new fields of applications, for which components have to possess a high fatigue resistance.
关键词： Hot isostatic pressing,Critical cooling rate,Additive manufacturing,Fatigue resistance,Laser powder-bed fusion,Selective laser melting
更新于2025-09-23 15:19:57
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Research on Post-processing Microstructure and Property of Titanium Components with Selective Laser Melting (SLM)
摘要： Additive manufacturing of titanium component holds promise to deliver benefit such as reduced cost, weight and carbon emissions during both manufacture and use. To capitalize on the benefits, it must be shown that the mechanical performance of parts produced by additive manufacturing can meet design requirement that are typically based on wrought material performance properties. Of particular concern for safety critical structures is the fatigue property of parts produced by additive manufacturing. Microstructure evolution, and its influence on mechanical properties of the alloy in the as-fabricated condition, has been documented by various researchers. However, fatigue crack propagation and the effects of the directional structure have not been sufficiently studied, imposing a barrier for this technology’s potential extension to high-integrity applications. In this study, fatigue life (S-N) and fatigue crack growth (FCG) both parallel and perpendicular to the build directions was studied. The interaction between the directional as-fabricated SLM microstructure and FCG was investigated and compared to that of the hot isostatic pressing (HIP) specimens with and without the stress relief after fabricating with SLM.
关键词： Titanium Components,Selective Laser Melting (SLM),Hot Isostatic Pressing (HIP),Fatigue Property,Microstructure
更新于2025-09-19 17:13:59
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Fabrication and Laser Performances of Yb:Sc2O3 Transparent Ceramics from Different Combination of Vacuum Sintering and Hot Isostatic Pressing Conditions
摘要： In this paper we report on the preparation and laser performance of transparent 3at.% Yb:Sc2O3 ceramics by reactive sintering of commercially available powders under vacuum followed by hot isostatic pressing (HIP). Combinations of different vacuum sintering temperatures (1650 °C and 1750 °C) and different HIP treatments (1700 °C and 1800 °C at 200 MPa) were tested in order to understand how these steps influence the microstructure and thus the optical and lasing properties of the ceramic samples. All the samples showed a good optical quality. The microstructure analysis and the laser tests showed that the vacuum pre-sintering temperature is the key factor determining the quality of the samples and the laser performances. The best values of slope efficiency i.e. ηL=50% and output power i.e. Pout=6.62 W were obtained for the sample pre-sintered under vacuum at 1650 °C and hot isostatically pressed at 1800 °C.
关键词： Yb-doped Sesquioxides Laser Ceramics,Laser Ceramics,Hot Isostatic Pressing
更新于2025-09-12 10:27:22
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Effect of Hot Isostatic Pressing on Al-10%Si-0.4%Mg Alloy Fabricated by Selective Laser Melting; レーザ積層造形により作製したAl-10%Si-0.4%Mg合金における熱間等方加圧処理の影響;
摘要： In this study, we investigated the effects of hot isostatic pressing (HIP) on the mechanical properties of an Al-10%Si-0.4%Mg alloy fabricated by selective laser melting (SLM). In addition, the effect of internal porosity on the mechanical properties of the alloy was also investigated. After the HIP, the internal porosity of the alloy decreased, while its elongation to failure (EL) improved significantly. However, the 0.2% proof stress (PS) and the tensile strength (TS) of the HIPed alloy were significantly lower than those of the as-built state. This can be attributed to the microstructural changes that occurred at elevated temperatures during the HIP. In addition, the PS and TS of the as-built alloy decreased with an increase in the internal porosity. On the other hand, in the case of the HIPed alloy, the PS and TS were not affected by the internal porosity. However, EL was sensitive to the internal porosity. The EL of the HIPed alloy decreased with an increase in its initial internal porosity. This is because the diffusion bonding during the HIP was imperfect owing to the presence of oxidized scales. Hence, it is imperative to optimize the laser irradiation conditions for the fabrication of aluminum alloy by SLM.
关键词： aluminum alloy,selective laser melting (SLM),hot isostatic pressing (HIP),additive manufacturing (AM),internal porosity
更新于2025-09-11 14:15:04
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Influence of heat treatment under hot isostatic pressing (HIP) on microstructure of intermetallic-reinforced tool steel manufactured by laser powder bed fusion
摘要： Microstructure and properties of as-built laser powder bed fusion (LPBF) steels differ from the conventional ones, and they may contain some porosity and lack of fusion. Therefore, post-treatments, including hot isostatic pressing (HIP), are used to densify the material, and tailor the properties of the final product. Usually, HIP is performed as an operation separate from heat treatment. In the present investigation a new approach was used, in which the whole cycle of the heat treatment was carried out in HIP under pressure, and the influence of HIP on microstructure of an advanced stainless maraging tool steel manufactured by LPBF was investigated. For a comparison, a conventional steel grade of the same chemical composition, after a heat treatment at the same temperature-time conditions, was also characterized. The microstructure of the steel was investigated by means of advanced microscopy and atom probe tomography. The influence of the manufacturing route, heat treatment and HIP on microstructure, austenitic phase fraction and size distribution of precipitates was investigated, and the role of high pressure in stabilization of austenite in the microstructure was discussed. It was concluded that since HIP influences phase transformations, a fundamental understanding of the influence of HIP on microstructure is necessary, and development of new post processing regimes guaranteeing the best performance of the material is required.
关键词： Hot isostatic pressing (HIP),Atom probe tomography,Transmission electron microscopy,Maraging steel,Precipitation hardening,Laser powder bed fusion
更新于2025-09-11 14:15:04
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Transparent tetragonal-cubic zirconia composite ceramics densified by spark plasma sintering and hot isostatic pressing
摘要： Targeting higher toughness transparent ceramics, tetragonal (3 mol % yttria) and cubic (8 mol % yttria) ZrO2 starting powder mixtures were densified by spark plasma sintering (SPS) in vacuum at 1100°C and post hot isostatic pressing (HIP) in argon at 1100°C. The influence of the ultra-fine microstructure and phase composition on the fracture resistance and light transmission in the visible and infra-red range was assessed. Of special interest was the influence of a thermal annealing step in air on the transparency of the SPS and SPS-HIP ceramics.
关键词： Total Forward Transmission,Hot Isostatic pressing,Spark Plasma Sintering,Ferro-elastic domain switching,Transparent zirconia
更新于2025-09-10 09:29:36