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Dopamine Binding and Analysis in Undiluted Human Serum and Blood by the RNA-Aptamer Electrode
摘要： Specific analysis of such neurotransmitters as dopamine by the aptamer electrodes in biological fluids is detrimentally affected by non-specific adsorption of media, particularly pronounced at positive charges of the electrode surface at which dopamine oxidizes. Here, we show that dopamine analysis at the RNA-aptamer/cysteamine-modified electrodes is strongly inhibited in undiluted human serum and blood due to non-specific interfacial adsorption of serum and blood components. We demonstrate that non-specific adsorption of serum proteins (but not of blood components) could be minimized when analysis is performed in a flow and injections of serum samples are followed by washing steps in a phosphate buffer solution (PBS) carrier. Under those conditions, the dopamine-aptamer binding affinity in whole human serum of (1.9±0.3)×104 M-1 s-1 was comparable to (3.7±0.3)×104 M-1 s-1 found in PBS, and the dopamine oxidation signal linearly depended on the dopamine concentration, providing the sensitivity of analysis of 73 ± 3 nA μM-1 cm-2 and the LOD of 114 ± 8 nM. The flow-injection apatmer-electrode system was used for direct analysis of basal levels of dopamine in undiluted human serum samples, without using any physical separators (membranes) or filtration procedures. The results suggest a simple strategy for combatting biosurface fouling most pronounced at positive electrode potentials and assist in designing more efficient antifouling strategies for biomedical applications.
关键词： Human serum,Blood,Surface fouling,RNA aptamer electrode,Dopamine,Chronoamperometry,Electrochemical Impedance,Flow-through cell
更新于2025-09-23 15:22:29
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Impedance Spectroscopy: A Versatile Technique to Understand Solution-Processed Optoelectronic Devices
摘要： Solution-processed optoelectronic devices based on conjugated polymers, colloidal quantum dots (CQDs), halide perovskites, and so on are now emerging as a new-generation semiconductor technology which prevails its conventional counterparts in terms of low fabrication cost, ease of scalable manufacturing, and abundant material designability. However, the solution-processed thin films obtained through spin-coating, spray, inkjet printing, and doctor blading usually suffer from low film quality and a high defect density especially at the interfaces of different functional layers. Currently, the most significant subject is to address the non-ideal interfaces for achieving improved performance of the devices. Impedance spectroscopy (IS) is a universal technique that can help to examine the charge behavior at the interfaces in an electrochemical or solid-state multilayered device. Owing to its ability to elucidate the charge transfer, charge transport, and accumulation within the interfaces of electrochemical or multilayered devices with minimal effects to the devices themselves, the use of IS has increased vividly in the last decades. This review provides the basic principles of IS and its applications on solution-processed optoelectronic devices.
关键词： optoelectronic devices,metal halide perovskites,quantum dots,impedance spectroscopy,solution processing
更新于2025-09-23 15:22:29
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Fabrication, electrical and magnetic properties of 0.7(BiGd <sub/>x</sub> Fe <sub/>1?x</sub> O <sub/>3</sub> )?0.3(PbTiO <sub/>3</sub> ) composites
摘要： The polycrystalline samples having chemical formula 0.7(BiGdxFe1?xO3)?0.3(PbTiO3) (x = 0.0, 0.05, 0.10, 0.15 and 0.20) were fabricated by using high temperature mixed oxide route. The X-ray diffraction spectra suggested rhombohedral (major) symmetry with small impurity phases. The surface microstructure showed a highly dense packing of grains throughout the wider area for all samples. The dielectric permittivity and loss factor of all samples were studied with the help of temperature-dependent dielectric parameters. The relaxation mechanism was suggested from the dielectric and impedance spectroscopy. The conduction mechanism of all samples was investigated. The P–E and M–H loops of all the samples were taken at room temperature showing the multiferroic properties.
关键词： Dielectric,conductivity,magnetic properties,ferroelectric,impedance
更新于2025-09-23 15:22:29
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Different Influence of Grid Impedance on Low- and High- frequency Stability of PV Generators
摘要： Recently, the stability issues when renewable energy sources are connected to weak grid have obtained great attention. The popular view thinks that the grid impedance is adverse to the system stability. However, in this paper, it is first found that for the photovoltaic (PV) generator, the grid impedance has different influence on the system stability depending on the frequency range when the complete model of the PV generator is taken into consideration. That is, the increase of grid impedance can suppress the low-frequency (<50 Hz) oscillation, while the increase of grid impedance degrades the high-frequency (>300 Hz) stability. Concretely, for the low-frequency range mainly dominated by the power loop and voltage loop of the PV generator, the describing function method is adopted to overcome discontinuity and nonlinearity of the power loop. Then, the low-frequency dynamics like power oscillation can be analyzed accurately. For the high-frequency range mainly dominated by the phase-locked loop and current loop of the PV generator, the impedance analysis method is adopted to reveal the high-frequency instability mechanism. Through these analyses, the different influence of grid impedance on the low- and high- frequency stability of PV generators can be clearly distinguished. All the conclusions are verified through the real-time hardware-in-loop (HIL) tests.
关键词： describing function,impedance analysis,PV generators,weak grid,stability analysis
更新于2025-09-23 15:22:29
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Characterization of the optical absorption, electric modulus, and thermal conductivity of poly(ethylene oxide) dispersed with alum and carbon black nanoparticles
摘要： Optical, electrical, and thermal properties of hybrid polymer thin films, made of poly(ethylene oxide) (PEO) filled with electrolyte alum salt of different concentrations, and doped with conductive carbon black (CB) nanoparticles (0.1 wt%), have been investigated. The optical properties were studied in the UV-visible wavelength range, thermal properties were studied as a function of temperature, filler content, and applied field frequency. The observed physical constants of the casted thin films like optical energy gap, energy tails, refractive index, thermal conductivity, impedance, dielectric constant, and electric modulus were determined. It was found that these measured quantities vary with the incident UV-wavelength, alum content, temperature and applied field frequency. The dependence of the electric modulus on frequency exhibit a relaxation peak occurs at 600 kHz.
关键词： Dielectric,Optical,Impedance,Thermal Conductivity,PEO,CB
更新于2025-09-23 15:22:29
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[IEEE 2018 9th International Conference on Ultrawideband and Ultrashort Impulse Signals (UWBUSIS) - Odessa, Ukraine (2018.9.4-2018.9.7)] 2018 9th International Conference on Ultrawideband and Ultrashort Impulse Signals (UWBUSIS) - Radiation Resistance of Resonant Impedance Monopole Placed on Metal Square Screen
摘要： The asymptotical solution of the 3-D vector problem of diffraction of the field of the monopole with the uniform distributed surface impedance, placed on the ideally conducting rectangular screen with the sides sizes L and W is obtained. Within the frame of the uniform geometrical theory of diffraction the radiation field in a far zone is represented as the sum of the geometric optics field from an impedance monopole placed on infinite screen, and the diffracted fields from the rectangular screen edges. The radiation resistances are calculated by the Poynting vector method as the functions of the monopole’s surface impedance and the sizes of monopole and screen. The input impedances of the same monopoles on the square screens have calculated using commercial software too. It is shown that at all surface impedances and monopole’s lengths the radiation and input resistances reach maximum at L=W=0.9 of wavelength.
关键词： impedance monopole,surface impedance,square screen,radiation resistance,input impedance,amplitude
更新于2025-09-23 15:21:21
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DIAMAGNETO-DIELECTRIC ANISOTROPIC WIDE ANGLE IMPEDANCE MATCHING LAYERS FOR ACTIVE PHASED ARRAYS
摘要： In this paper, we present the full process of designing anisotropic metamaterial (MM) wide angle impedance matching (WAIM) layers. These layers are used to reduce the scan losses that occur in active phased arrays for large scanning angles. Numerical results are provided to show the improvement in performances that such layers can ensure. The proposed anisotropic MM-WAIM layers achieve an improvement of about 1 dB of more radiated power at θ = 70? from broadside, in a 13% of fractional bandwidth on the azimuthal plane φ = 90?. Weaker improvements are obtained in the other azimuthal planes, however keeping the active re?ection coe?cient below ?9 dB for all azimuthal planes up to θ = 60? and up to θ = 70? o?-axis for planes φ = 45?, 90? in the whole operational band.
关键词： scan losses,wide angle impedance matching,anisotropic metamaterial,active phased arrays,impedance matching
更新于2025-09-23 15:21:21
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[IEEE 2018 9th International Conference on Ultrawideband and Ultrashort Impulse Signals (UWBUSIS) - Odessa, Ukraine (2018.9.4-2018.9.7)] 2018 9th International Conference on Ultrawideband and Ultrashort Impulse Signals (UWBUSIS) - Combined Wide-Angle Scanning by a Two-Dimensional Dipole Array
摘要： An analytical solution of an impedance synthesis problem for a two-dimensional dipole antenna array is obtained. The array consists of thin impedance electric dipoles whose centers are located at nodes of a planar rectangular grid with double periodicity. Radiation patterns of each dipole in the array does not differ from that of an isolated dipole. A new method for wide-angle scanning of the array radiation pattern, combining the simultaneous variation of phases of the excitation currents in the dipoles and of their surface impedances is proposed.
关键词： thin impedance dipole,flat two-dimensional antenna array,wide-angle scanning,radiation pattern,wave zone,impedance synthesis method
更新于2025-09-23 15:21:21
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A new dual band 4 x 4 butler matrix with dual band 3dB quadrature branch line coupler and dual band 45° phase shifter
摘要： A new dual band 4 × 4 butler matrix (BM) without crossover has been proposed, implemented and analyzed in this paper. A new dual band 45° phase shifter has also been proposed. The dual band BM, dual band 3dB quadrature branch line coupler (BLC) and dual band 45o phase shifter have been designed using Keysight Technologies’ Advanced Design System (ADS) software and implemented on the Rogers 2.33, having a thickness of 0.787 mm for 1.0 GHz and 2.5 GHz operating frequencies. Before the implementation of the proposed BM, the dual band 3dB quadrature BLC and dual band 45° phase shifter have been designed, implemented and analyzed. The proposed dual band 4 × 4 BM has been developed by placing four dual band 3dB quadrature BLCs and two dual band 45° phase shifters at their appropriate positions. Circuit parameters variation of the proposed BLC, phase shifter and BM with frequency ratios have been studied in this paper. The measured and simulated results of the dual band BM validated the design methodology. A performance analysis comparing the proposed BM with the existing butler matrices has also been carried out.
关键词： branch line coupler,Butler matrix,dual band,impedance transformer,45o phase shifter,advanced design system
更新于2025-09-23 15:21:21
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Magnetoelectric uniaxial metamaterials as wide-angle polarization-insensitive matching layers
摘要： Antire?ection or impedance matching is a topic that has been extensively researched by the optical and microwave communities over the past century and until today. However, due to the diverging wave impedances of TE (s) and TM (p) polarizations with increasing incident angle, it is impossible to achieve perfect matching simultaneously for both polarizations at varying incidence angles with a single conventional isotropic matching layer. To achieve polarization-insensitive matching at an arbitrary incident angle, we propose a magnetoelectric uniaxial metamaterial layer (MEUML) that is inspired by the perfectly matched layer (PML) concept in computational electromagnetics. Similar to the PML, the MEUML requires speci?c uniaxial permittivity and permeability tensors. However, to simultaneously control both the transversal and longitudinal material parameters is not an easy task. To date, a true PML has not been realized with metamaterials. In this paper, we employ a simple and yet special metamaterial unit cell to achieve such control and synthesize a physical MEUML. The unit cell comprises two parallel metallic rings separated by a holey substrate. The transversal electric and magnetic dipole moments, and the longitudinal capacitive and diamagnetic coupling between the rings are judiciously controlled to achieve the required permittivity and permeability tensors. To aid the MEUML synthesis, we also introduce a technique that can extract the material parameter tensors at any incident angle. We ?rst demonstrate this concept by achieving polarization-insensitive matching of a high-index substrate at 45? with a single subwavelength-thick MEUML. We further adapt the concept to the microwave regime by developing a MEUML-based radome. Exceptional matching performance was obtained both in the simulations and measurements. The re?ectance remains below 5% from normal incidence (0?) to near grazing angle (85?) for both polarizations and over a wide bandwidth. With this unprecedented control of the material parameter tensors, the MEUML concept not only can be applied to impedance matching, but also can be utilized in many exotic applications that require extreme control of the material properties.
关键词： wide-angle,impedance matching,polarization-insensitive,radome,magnetoelectric uniaxial metamaterials
更新于2025-09-23 15:21:21