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PZT/PZT and PZT/BiT Composite Piezo-Sensors in Aerospace SHM Applications: Photochemical Metal Organic + Infiltration Deposition and Characterization
摘要： The composition of fine-ground lead zirconate-titanate powder Pb(Zr0.52Ti0.48)O3, suspended in PZT and bismuth titanate (BiT) solutions, is deposited on the curved surface of IN718 and IN738 nickel-based super alloy substrates up to 100 μm thickness. Photochemical metal organic and infiltration techniques are implemented to produce smooth, semi-dense, and crack-free random orientated thick piezoelectric films as piezo-sensors, free of any dopants or thickening polymers. Every single layer of the deposited films is heated at 200 °C with 10 wt.% excess PbO, irradiated by ultraviolet lamp (365 nm, 6 watt) for 10 min, pyrolyzed at 400 °C, and subsequently annealed at 700 °C for one hour. This process is repeated successively until reaching the desired thickness. Au and Pt thin films are deposited as the bottom and top electrodes using evaporation and sputtering methods, respectively. PZT/PZT and PZT/BiT composite films are then characterized and compared to similar PZT and BiT thick films deposited on the similar substrates. The effect of the composition and deposition process is also investigated on the crystalline phase development and microstructure morphology as well as the dielectric, ferroelectric, and piezoelectric properties of piezo-films. The maximum remnant polarization of Pr = 22.37 ± 0.01, 30.01 ± 0.01 μC/cm2, the permittivity of εr = 298 ± 3, 566 ± 5, and piezoelectric charge coefficient of d33 = 126, 148 m/V were measured versus the minimum coercive field of Ec = 50, 20 kV/cm for the PZT/PZT and PZT/BiT thick films, respectively. The thick film piezo-sensors are developed to be potentially used at frequency bandwidth of 1–5 MHz for rotary structural health monitoring and also in other industrial or medical applications as a transceiver.
关键词： piezoelectric sensor,structural health monitoring,PZT/BiT,composite,characterization,sol-gel PMOD deposition,infiltration,aerospace structure,PZT/PZT,thick film
更新于2025-09-23 15:22:29
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Tunable Low Power Piezo-Plasmonic Random Laser under External Voltage
摘要： This study was aimed to introduce a new kind of low power and tunable random lasers based on piezo-plasmonic core/shell nanoparticles (NPs) consisting of lead zirconate titanate and gold, mixed by different concentrations of Rhodamine B (RhB) dye. To get the random lasing, the sample was exposed to pulsed laser at the presence and in the absence of an external voltage. We got a gradual increase in the thermo-plasmonic emission intensity was enhanced by decreasing the threshold lasing due to an increase in scattering, which more easily made a close loop path in the gain medium. Our results showed some spikes with the same pump energy in emission spectrum which confirmed the coherence random lasing. This phenomenon could be observed in PZT@Au NPs and it could not be observed in Au@PZT NPs in low and high concentrations. properties by increasing the applied voltage on core/shell NPs, which depended on the boundary conditions between the shell and the core samples. By external voltage, the Furthermore, in lower pump energy, we observed low peak intensity in the emission spectrum and it increased as the pump energy overrode the lasing threshold. The emission spectrum became narrow with a sharp increase in the emission intensity, which we could reach a rapid decrease in the full width at half maximum (FWHM) of the emission intensity above the threshold. These results showed the possibility of using these new kinds of materials for low threshold and controllable random lasing.
关键词： external voltage,thermo-plasmonic,piezo-plamsonic,random laser,Au@PZT,PZT@Au core/shell NPs
更新于2025-09-19 17:13:59