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oe1(光电查) - 科学论文

17 条数据
?? 中文(中国)
  • Color Reproduction Accuracy Promotion of 3D-Printed Surfaces Based on Microscopic Image Analysis

    摘要: Full-color 3D printing technology is a powerful process to manufacture intelligent customized colorful objects with improved surface qualities; however, poor surface color optimization methods are the main impeding factors for its commercialization. As such, the paper explored the correlation between microstructure and color reproduction, then an assessment and prediction method of color optimization based on microscopic image analysis was proposed. The experimental models were divided into 24-color plates and 4-color cubes printed by ProJet 860 3D printer, then impregnated according to preset parameters, at last measured by a spectrophotometer and observed using both a digital microscope and a scanning electron microscope. The results revealed that the samples manifested higher saturation and smaller chromatic aberration (ΔE) after post-processing. Moreover, the brightness of the same color surface increased with the increasing soaked surface roughness. Further, reduction in surface roughness, impregnation into surface pores, and enhancement of coating transparency effectively improved the accuracy of color reproduction, which could be verified by the measured values. Finally, the chromatic aberration caused by positioning errors on different faces of the samples was optimized, and the value of ΔE for a black cube was reduced from 8.12 to 0.82, which is undetectable to human eyes.

    关键词: Structural characterisation,Impregnating process,Scanning electron microscope,Image analysis,Color optimization,Full-color printing

    更新于2025-11-21 11:18:25

  • Alignment of liquid crystals using Langmuir?Blodgett films of unsymmetrical bent-core liquid crystals

    摘要: The properties of the thin films of liquid crystal (LC) molecules can be governed easily by external fields. The anisotropic structure of the LC molecules has a large impact on the electrical and optical properties of the film. The Langmuir monolayer (LM) of LC molecules at the air–water interface is known to exhibit a variety of surface phases which can be transferred onto a solid substrate using the Langmuir?Blodgett (LB) technique. Here, we have studied the LM and LB films of asymmetrically substituted bent-core LC molecules. The morphology of LB film of the molecules is found to be a controlling parameter for aligning bulk LC in the nematic phase. It was found that the LB films of the bent-core molecules possessing defects favour the planar orientation of nematic LC, whereas the LB films with fewer defects show homeotropic alignment. The defect in LB films may introduce splay or bend distortions in the nematic near the alignment layer which can govern the planar alignment of the bulk LC. The uniform layer of LB film facilitates the molecules of nematic to anchor vertically due to a strong van der Waals interaction between the aliphatic chains leading to a homeotropic alignment.

    关键词: field emission scanning electron microscope,atomic force microscope,Langmuir?Blodgett film,liquid crystals,Brewster angle microscopy,Langmuir monolayer

    更新于2025-11-21 11:01:37

  • [IEEE 2018 15th International Conference on Control, Automation, Robotics and Vision (ICARCV) - Singapore, Singapore (2018.11.18-2018.11.21)] 2018 15th International Conference on Control, Automation, Robotics and Vision (ICARCV) - Detection and Compensation of Motion Error for Nanomanipulation Platform in Scanning Electron Microscope

    摘要: Nanomanipulation system based on scanning electron microscope(SEM) with good real-time visual feedback and nanoscale observation resolution had high operability in a vacuum working environment. Different nanomanipulation tasks of carbon nanotubes (CNTs) are carried out through the nanomanipulation system in SEM. Nanomanipulation platform existed inherent manufacture errors, installation errors and other errors, and imprecise nanomanipulation system were also time-consuming and laborious for operators. This paper presentes a method of combining the visual feedback and feedforward control to detect and compensate the motion error of the multi-dimensional SmarAct nanomanipulation platform in the nanomanipulation system in SEM. This method reduces the motion error in the X-Y direction and achieved higher operating accuracy. At the different step speed, the motion error in the X direction and Y direction is 135.7nm and 112.9nm respectively. After the feedforward compensation, the motion error in the X direction and Y direction reduces to 61.3nm and 54.1nm respectively.

    关键词: feedforward control,Scanning Electron Microscope (SEM),visual feedback,nanomanipulation

    更新于2025-09-23 15:23:52

  • Effect of thickness and post deposition annealing temperature on the structural and optical properties of thermally evaporated molybdenum oxide films

    摘要: In this paper, the influence of thickness and post deposition annealing temperature on thermally evaporated molybdenum oxide films has been studied. The X-ray diffraction (XRD) and Scanning Electron Microscope (SEM) are used for crystal structural and surface morphological characterization of the films, respectively. The XRD analysis showed that the presence of α-MoO3 and MoO2 crystalline phase of the films annealed at elevated temperature ~ 250 °C after deposition. The optical constants are determined from UV–Vis transmission spectra. The optical band gap and Urbach energy is found to be temperature dependent. The refractive index of the films is estimated by the optical method as well as cross-sectional SEM image analysis. It is found that the refractive index of the films increases from ~ 1.70 to 2.03 with the decrease in film thickness from ~ 2.9 to 1.7 μm. It is also observed that the refractive index decreased from ~ 2.03 to 1.61 with the increase in post deposition annealing temperature from room temperature (RT) to ~ 250 °C. Moreover, extinction coefficient, optical conductivity, porosity, and film density are investigated as a function of source-substrate distance and post deposition annealing temperature. The Photoluminescence (PL) properties of the films are also investigated by recording spectra under the excitation wavelength at 250 nm.

    关键词: Optical constants,Molybdenum oxide,X-ray diffraction,Thermal evaporation,Scanning electron microscope

    更新于2025-09-23 15:22:29

  • Temperature effect on structural, optical and NH<SUB align="right">3 gas sensing properties of TeO<SUB align="right">2 thin films

    摘要: TeO2 thin films with different temperatures (400, 450 and 500°C) were deposited on glass substrates by thermal evaporation technique from a Te powder. XRD patterns indicate that as the temperature increases, the crystallisation improves. Observing the images obtained by SEM, it is seen that the grain size decreases as the temperature increases. The optical energy gap of the films was determined from transmittance and reflectance spectra. The optical energy gap decreased continuously from 3.95 eV to 3.80 eV with increasing temperature. Studying the effect of deposition temperature on NH3 gas measurement, it became obvious that as the deposition temperature increases, the sensitivity increases and the response and recovery times decrease.

    关键词: scanning electron microscope,XRD,thin films,sensitivity,X-ray diffraction,energy gap,SEM,optical

    更新于2025-09-23 15:22:29

  • Characterisation of elemental analysis, carbon sulphur analysis and impact test of stent manufacturing using medical grade ASTM F75 cobalt chromium (CoCrMo) by selective laser melting (SLM) technology

    摘要: This paper explains and demonstrates the capabilities of metal additive manufacturing (MAM) technology in producing intricate stent structure with a customise design by using ASTM F75 cobalt chromium powder. The elemental analysis (EDX-SEM), carbon sulphur analysis and Impact Test are being develop and tested and thus exploring the potential area of MAM process for future proof stent manufacturing. By alternatively switching to MAM, the step of production can be minimised and thus customisation of stent can be carried out according to the patient’s need. The suggested model of the stent was taken from the third-party vendor and fabrication was carried out using EOSINT M280 metal printer with the aid of Materialise Magics 19.0 software for support generation.

    关键词: stent,scanning electron microscope (SEM),selective laser melting (SLM),cobalt chromium (CoCrMo),energy-dispersive X-ray spectroscopy (EDX),Metal additive manufacturing (MAM)

    更新于2025-09-23 15:21:01

  • Mapping Local Surface Plasmon Modes in a Nanoplasmonic Trimer Using Cathodoluminescence in the Scanning Electron Microscope

    摘要: The excitability of local surface plasmon modes in radial trimers composed of gold nanorods was mapped using hyperspectral cathodoluminescence (CL) in the scanning electron microscope. In symmetric trimers, the local plasmon resonances could be excited most effectively at the ends of individual rods. Introducing asymmetry into the structure breaks the degeneracy of the dipole modes and changes the excitability of transverse dipole modes in different directions. CL in the scanning electron microscope has great potential to interrogate individual nanophotonic structures and is a complement to electron energy loss spectroscopy and optical microscopy.

    关键词: scanning electron microscope,local surface plasmon mode,nanoplasmonic trimer,cathodoluminescence

    更新于2025-09-23 15:21:01

  • Highly Rectifying Heterojunctions Formed by Annealed ZnO Nanorods on GaN Substrates

    摘要: We study the effect of thermal annealing on the electrical properties of the nanoscale p-n heterojunctions based on single n-type ZnO nanorods on p-type GaN substrates. The ZnO nanorods are prepared by chemical bath deposition on both plain GaN substrates and on the substrates locally patterned by focused ion beam lithography. Electrical properties of single nanorod heterojunctions are measured with a nanoprobe in the vacuum chamber of a scanning electron microscope. The focused ion beam lithography provides a uniform nucleation of ZnO, which results in a uniform growth of ZnO nanorods. The specific configuration of the interface between the ZnO nanorods and GaN substrate created by the focused ion beam suppresses the surface leakage current and improves the current-voltage characteristics. Further improvement of the electrical characteristics is achieved by annealing of the structures in nitrogen, which limits the defect-mediated leakage current and increases the carrier injection efficiency.

    关键词: chemical bath deposition,nanoscale heterojunctions,ZnO nanorods,nanoprobe in the scanning electron microscope,current-voltage characteristics,annealing,focused ion beam patterning

    更新于2025-09-23 15:19:57

  • A Beginners' Guide to Scanning Electron Microscopy || Imaging with the SEM

    摘要: The scanning electron microscope is routinely used to characterize wide-ranging materials due to its ease of operation and relatively straightforward sample preparation as well as due to simple image interpretation. New users can readily obtain images after little practice. However, high-resolution microscopy and examination of “difficult” samples require experience and know-how of the principles of image formation in the SEM. This chapter describes the role of various operational parameters used during microscopy in more detail. The effect of these parameters on contrast, resolution, and depth of field depicted by images is discussed. Pros and cons of microscopy conditions that have a direct bearing on the quality of images, type of information obtained, and image interpretation are elaborated. Guidelines for operation and upkeep of the SEM instrument are also summarized in this chapter.

    关键词: high-resolution microscopy,operational parameters,resolution,scanning electron microscope,SEM,image formation,contrast,microscopy conditions,image interpretation,depth of field

    更新于2025-09-23 15:19:57

  • New process of tempering color printed glass by using laser irradiation

    摘要: Colored glass products with various printing technologies are becoming more important in industry. The aim is to achieve individual solution in a very short delivery time. Conventional thermal treatment of burning glasses in oven for tempered color printing has predominant issues with high time consumption, energy consumption and manufacturing cost. It requires alternative process development. This paper proposes laser process to overcome issues in conventional treatment with the latest results of tempering colored glass. Samples have been analyzed with the scanning electron microscope (SEM). Two different laser systems have been applied and the glass has been printed with black paste.

    关键词: scanning electron microscope (SEM),glass,printing technologies,laser material processing,pigment paste,surface treatment

    更新于2025-09-12 10:27:22