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Computational and Experimental Investigation of Micro-Hardness and Wear Resistance of Ni-Based Alloy and TiC Composite Coating Obtained by Laser Cladding
摘要： The influence of processing parameters on the micro-hardness and wear resistance of a Ni-based alloy and titanium carbide (TiC) composite cladding layer was studied. Mathematical models were developed to predict the micro-hardness and wear resistance of the cladding layer by controlling the laser cladding processing parameters. Key processing parameters were the laser power, scanning speed, gas flow, and TiC powder ratio. The models were validated by analysis of variance and parameter optimization. Results show that the micro-hardness is positively correlated with laser power and TiC powder ratio, where the TiC powder ratio shows the most significant impact. The wear volume decreased with an increasing TiC powder ratio. The targets for the processing parameter optimization were set to 62 HRC for micro-hardness and a minimal volume wear. The difference between the model prediction value and experimental validation result for micro-hardness and wear volume were 1.87% and 6.33%, respectively. These models provide guidance to optimize the processing parameters to achieve a desired micro-hardness and maximize wear resistance in a composite cladding layer.
关键词： Ni35A + TiC composite,laser cladding,central composite design,wear resistance,micro-hardness
更新于2025-11-28 14:24:20
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Control and prediction of forming quality in curved surface multi-track laser cladding with curve paths
摘要： This research investigated the influence of different processing parameters in curved surface multi-track laser cladding with curve paths. Mathematical models of flatness ratio, incomplete fusion, and pore area in the clad were developed by central composite design with altering the input laser power, scanning speed, gas flow, and overlapping rate. Response surface methodology was used to analyze the correlation of different processing parameters affecting the selected responses. A clad with better flatness ratio was achieved by properly increasing the laser power and gas flow while reducing the overlapping rate. Appropriately increasing the laser power and overlapping rate while reducing the scanning speed and gas flow effectively diminished the incomplete fusion. Less pore area in the clad was obtained by appropriately increasing the laser power and overlapping rate while reducing the scanning speed and gas flow. Afterwards, desired processing parameters set was obtained by the optimization with the target of maximizing the flatness ratio and also minimizing the incomplete fusion and pore area. Experimental validation with this processing parameter setup provided satisfactory clad, and the error rate for the flatness ratio, incomplete fusion, and pore area was 1.708%, 5.714%, and 6.522%, respectively. This paper provides the theoretical guidance for the prediction and control of the flatness ratio, incomplete fusion, and pore area in curved surface multi-track laser cladding with curve paths.
关键词： Central composite design,Response surface methodology,Curved surface,Laser cladding
更新于2025-09-19 17:13:59
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Investigation of Geometric Characteristics in Curved Surface Laser Cladding with Curve Path
摘要： Laser cladding on curved surfaces is essential in industrial applications for restoration and remanufacturing of high-value parts. This study investigated the in?uence of di?erent factors on clad width, clad height, and dilution rate in curved surface laser cladding with curved path. Mathematical models were developed using central composite designs to predict these geometric characteristics by controlling laser power, scanning speed, gas ?ow, and altering the outside radius of the cylindrical substrate. Analysis of variance and response surface methodology indicated that clad width increased with increasing laser power and reducing scanning speed. Clad height positively correlated to laser power and negatively correlated to the outside radius of the cylindrical substrate. Increasing the laser power while decreasing the scanning speed led to an increase in dilution rate. Afterwards, the geometric characteristics of the clad were improved by optimizing these factors with the target to maximize clad width and height as well as to minimize dilution rate. The di?erence between model predictions and experimental validations for clad width, clad height, and dilution rate were 3.485%, 3.863%, and 6.566%, respectively. The predicted accuracy was veri?ed with these models, and they were able to provide theoretical guidance to predict and control the geometric characteristics of curved surface laser cladding with a curved path.
关键词： central composite design,curved surface,forming control,curve path,laser cladding
更新于2025-09-16 10:30:52
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Central Composite Design (CCD) Optimized Synthesis of Fe3O4@SiO2@AgCl/Ag/Ag2S as a Novel Magnetic Nano-Photocatalyst for Catalytic Degradation of Organic Pollutants
摘要： In this study, we formulated and synthesized an efficient visible light-active magnetic nano-photocatalyst, Fe3O4@SiO2@AgCl/Ag/Ag2S, to decompose methyl orange (MO) as a model organic pollutant. XRD, SEM, TEM, EDS, DRS, and VSM analyses were used to characterize the developed magnetic nano-photocatalyst. Moreover, central composite design (CCD) modeling, which is based on response surface methodology (RSM) modeling, is utilized to optimize the synthetic and operating conditions to maximize the photocataytic performance. The CCD-optimized values for molar ratio of AgCl to Fe3O4, molar ratio of Ag2S to Fe3O4, and the photocatalyst dosage are found to be 0.8, 0.27, and 1.27 g/L, respectively. The developed Fe3O4@SiO2@AgCl/Ag/Ag2S nano-photocatalyst shows a superior photocatalytic activity in decomposition of MO, degrading around 90% and 99% of MO in 30 min and one hour, respectively, under visible light illumination, at which the predicted values are in a good agreement with the experimental values (R2=0.971 and Adj-R2=0.945). Meanwhile, the morphological, physicochemical, and magnetic properties of the developed nano-photocatalyst are largely retained over ten successive cycles of photocatalytic reactions, and no significant decline in the photocatalytic activity is observed.
关键词： Magnetic Nano-Photocatalyst,Central Composite Design (CCD),Organic Pollutant,AgCl/Ag/Ag2S,Water Treatment
更新于2025-09-10 09:29:36
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Optimization of photocatalytic degradation of dye?wastewater?by CuFe<sub>2</sub>O<sub>4</sub>/AgBr composite using response surface methodology
摘要： In this paper, a simple response surface methodology (RSM) based on central composite design (CCD) was applied to determine the optimum processing parameters of photocatalytic degradation of acid red 88 (AR88) by CuFe2O4/AgBr composites. The effect of CuFe2O4 loading, initial concentration of pollutant, and photocatalyst concentration on the yield of AR88 degradation rate was investigated. Based on the statistical experimental design, the maximum degradation rate of 94.7% was achieved under optimal conditions: the 34.69% of CuFe2O4 loading, 16.34mg/L of intial concentration of AR88, 1.51g/L of photocatalyst concentration. The kinetics exploration indicated that the degradation process fitted pseudo-first order kinetic model. What’t more, the trapping experiment of active species demonstrated that ·O2- and ·OH were the dominant species.
关键词： CuFe2O4/AgBr composites,response surface methodology,central composite design,acid red 88,photocatalysis
更新于2025-09-04 15:30:14
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Optimization and modeling of UV-TiO <sub/>2</sub> mediated photocatalytic degradation of golden yellow dye through response surface methodology
摘要： In this article, heterogeneous photocatalysis of golden yellow (GY) dye by Evonik p25 titanium dioxide (PTD) and UV radiations was optimized by using central composite design of response surface methodology. The GY dye photocatalysis was expressed as the function of amount of PTD loading (X1), GY dye initial concentration (X2), and UV irradiance intensity (X3). The optimization of degradation conditions was done by measuring two different responses, that is, color removal (Y1) and chemical oxygen demand removal (Y2). The effect of X1, X2, and X3 were studied in the range 0.5–1.5 g/L, 15–35 W/m2, and 10–30 mg/L, respectively. The quadratic model was suggested for Y1 and Y2. The numerical optimization of results was done via Design Expert software. The predictive results obtained were verified by performing actual experiments. The photodegradation kinetics, total organic carbon disappearance, effect of inorganic salts, and H2O2 concentration on GY dye photodegradation were also studied.
关键词： Titanium dioxide,Heterogeneous photocatalysis,Central composite design,Optimization,Golden yellow dye,Response surface methodology
更新于2025-09-04 15:30:14