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Synthesis of Graphene Oxide Nanosheets via Modified Hummers’ Method and Its Physicochemical Properties
摘要： The efficient synthesis of exfoliated graphene oxide nanosheets (GO) via modified Hummers’ method was successfully carried out. The physicochemical properties of GO were determined by Fourier transform infrared spectroscopy (FTIR), UV-visible spectrophotometry (UV-vis), x-ray diffraction analysis (XRD), Raman spectroscopy, and transmission electron microscopy (TEM). The graphite was fully oxidized by strong oxidizing agent caused the oxygen-containing functional groups such as C-O-C, C=O, and COOH were introduced into the graphite layers as analyzed by Raman and FTIR. XRD pattern of GO showed 2θ of 12.0o with interlayer spacing ~ 7.37A which describe non uniform crystal structure with the addition of oxygen containing functional groups. UV-vis spectrum of GO exhibit maximum absorption peak at ~ 234 nm corresponding to the aromatic C=C bond with π-π* transition. The morphology of GO was observed to have flake-like shape and less transparent layers by TEM. The properties of synthesized GO suggest high potential in producing the high quality of graphene which is can be applied as the electrocatalyst support for direct methanol fuel cell application.
关键词： Graphene oxide nanosheets,characterization,Hummers’ method,graphite,chemical oxidation
更新于2025-09-23 15:22:29
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A simple and green synthesis of carbon quantum dots from coke for white light-emitting devices
摘要： Coke is a by-product of coal. This paper reports a simple and green chemical oxidation method for carbon quantum dots (CQDs) from coke for use in novel applications. The CQDs emit blue fluorescence and have a fluorescence quantum yield of 9.2% and blue-green-red spectral composition of 48%. A light-emitting diode (LED) was fabricated by combining the CQDs as a white-light converter with an ultraviolet chip. The Commission Internationale de L'Eclairage chromaticity coordinate (0.31, 0.35) and correlated color temperature (5125 K) of the LED are located in a cool white light zone, suggesting that they have superior potential application in lighting devices.
关键词： carbon quantum dots,white light-emitting devices,fluorescence,coke,chemical oxidation
更新于2025-09-16 10:30:52