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Interface characterization and mechanical properties of dual beam laser welding-brazing Al/steel dissimilar metals
摘要： The DP590 steel to AA7075 Al-alloy with lap configuration is successfully joined by dual beam laser welding-brazing without using filler metal. Through the introduction of the derived laser beam, the wetting angle, wetting distance and the thickness of intermetallic compound (IMC) layer are well improved and controlled. It is found that the wettability of liquid Al on steel improves with the increase of laser power, i.e. the wetting angle decreasing from 25.3° to 17.8° and the wetting distance increasing from 2.17 mm to 3.19 mm as the laser power increasing from 1.0 kW to 1.6 kW. Two kinds of IMC exist at brazing interface, one is η-phase (Fe2Al5) with flatten morphology closing to the steel side and the other is θ-phase (FeAl3) with needle-like morphology adjacent to the welding-brazing seam. The thickness of IMC layer increases from 8.37 μm to 12.12 μm with increasing laser power from 1.0 kW to 1.6 kW. Tensile test shows that both the wettability and the IMC thickness have influence on the welding-brazing joint strength. Poor wettability and too thick IMC layer will result in lower strength and fracture occurred in brazing interface. The optimal joint tensile strength of 123.7 MPa on average is achieved with the laser power of 1.4 kW.
关键词： Tensile strength,Welding-brazing,IMC,Dual beam laser,Al/steel dissimilar metals
更新于2025-11-28 14:24:20
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Laser and hybrid laser welding of type 316L(N) austenitic stainless steel plates
摘要： The effect of laser, Hybrid Laser-Tungsten inert gas (HLT) and Hybrid Laser-Metal inert gas (HLM) welding processes on the microstructure and mechanical properties of 5.6 mm thick 316L(N) stainless steel weld joints have been studied. The differences in weld metal microstructure and mechanical properties of the weld joints were evaluated and discussed. Weld bead geometry, ferrite number (FN), solidification mode, secondary dendrite arm spacing, hardness and tensile properties are compared. Laser weld joint showed narrow weld bead profile and a higher cooling rate than the hybrid laser arc weld joints and the weld metal manifested austenitic solidification mode. HLT weld displayed coarser weld metal microstructure due to higher heat input and austenitic ferritic solidification mode. HLM process possesses moderate heat input and cooling rate. The HLM weld metal exhibited ferritic austenitic solidification mode and 2.5 FN. The hardness of weld metal was higher in hybrid welding processes due to the higher ferrite content. HLM weld joint has higher yield strength, ultimate tensile strength and ductility compared to that of the other weld joints. HLM welding process also permits higher gap tolerance with filler metal addition and is recommended for welding of type 316L(N) stainless steel.
关键词： ferrite,stainless,welding,microstructure,steel,Laser,hybrid,solidification,316L(N),arc
更新于2025-11-21 11:24:58
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Complementary use of pulsed and continuous wave emission modes to stabilize melt pool geometry in laser powder bed fusion
摘要： The most common defects in laser powder bed fusion (LPBF) namely porosity, geometrical errors, roughness and thermal deformations are principally linked with the energy input to the process. In common practice, a single set of process parameters is used to produce a whole component independently from the dimensions of the actual scan path within a given layer. However, melt pool stability is highly dependent on the scanned geometry. A possible strategy to maintain a constant melt pool is the mixed use of pulsed wave (PW) and continuous wave (CW) emission regimes. Accordingly, this work investigates the complementary use of continuous and modulated emission at fixed energy density on large and thin sections respectively. The proposed approach is tested on AISI 316L stainless steel and melt pool observations are conducted employing a coaxial monitoring system built for purpose. Temporally resolved measurements of intensity and geometrical properties of the melt pool were extracted as well as a three-dimensional spatial mapping of the molten pool area. The results demonstrate that moving from CW to a PW regime at the transition zones to thinner sections is effective in maintaining a constant melt pool size thus avoiding heat build-up and part extrusion from the powder bed.
关键词： Selective laser melting,Stainless steel,Molten pool monitoring,CW emission,PW emission
更新于2025-11-14 15:24:45
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Microstructure and tribological properties of laser cladded self-lubricating nickel-base composite coatings containing nano-Cu and h-BN solid lubricants
摘要： In the present work, nickel-base composite powder (Ni60), nickel-base composite powder with the addition of h-BN solid lubricants (h-BN/Ni60) and nickel-base composite powder with the addition of nano-Cu encapsulated h-BN solid lubricants (nano-Cu/h-BN/Ni60) were used as raw materials to synthesize three different coatings on Q235 steels by laser cladding. Microstructures of these coatings were analyzed by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and Raman spectroscopy. Tribological properties of these coatings were investigated at the temperatures from 25 °C to 600 °C. High temperature micro-hardness measurement was performed by Vickers micro-hardness tester. The results showed that the h-BN particles survived after laser cladding and displayed a homogeneous distribution in the nickel-base composite matrix. The encapsulation of h-BN by nano-Cu resulted in an increase of h-BN content in the coating. Although the addition of nano-Cu and h-BN led to a decrease on hardness, the nano-Cu/h-BN/Ni60 coating had the lowest friction coefficient and wear rate among the three coatings in a wide range of temperature from 25 °C to 500 °C. The mechanism of wear reduction by addition of nano-Cu encapsulated h-BN solid-lubricants was also discussed in this research.
关键词： Laser cladding,Self-lubricant coating,Steel substrate,Wear,Wide temperature range,Nickel-base composite
更新于2025-09-23 15:23:52
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AIP Conference Proceedings [Author(s) 4TH ELECTRONIC AND GREEN MATERIALS INTERNATIONAL CONFERENCE 2018 (EGM 2018) - Bandung, Indonesia (27–28 July 2018)] - The enhancement of the corrosion protection of 304 stainless steel using Al2O3 films by PLD method
摘要： The enhancement of the corrosion protection of 304 stainless steel using Al2O3 films by PLD method. In this manuscript, we are using PLD to reduce the corrosion rate of the stainless steel 304 in hydrochloric acid with the concentration of 1 M and the immersion time of 4 minutes at room temperature. This method opens prospects to use the enhanced stainless steel for many electronics and manufacturing applications.
关键词： PLD,corrosion,Al2O3 films,304 stainless steel
更新于2025-09-23 15:23:52
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Drag reduction effect of ultraviolet laser-fabricated superhydrophobic surface
摘要： Superhydrophobic (SH) surface has been found effective for drag reduction in wall-bounded turbulence for decades, especially the metallic durable SH surfaces are believed very promising for improving the velocity and voyage of marine vehicles. We present stainless steel SH surfaces with U-groove patterns that fabricated by ultraviolet laser texturing and coating modifier treatment. The drag-reducing effects of the SH surfaces are tested by a self-built gravity sliding speed improving evaluation device. The results show that the different drag-reduction performance of the SH surfaces can be achieved by adjusting the line spacing of the crossing U-groove patterns. With the line spacing equalling to 80 μm, the ultraviolet laser textured stainless steel SH surface acquires the static contact angle of 161.5° and the dynamic sliding angle of only 2°, which leads to the maximum speed improving rate of 29.7%.
关键词： drag reduction,Superhydrophobic surface,stainless steel,laser texturing
更新于2025-09-23 15:23:52
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Signal enhancement in laser diode thermal desorption-triple quadrupole mass spectrometry analysis using microwell surface coatings
摘要： Laser diode thermal desorption (LDTD) is an ionization source usually coupled to triple quadrupole mass spectrometry (QqQMS) and specifically designed for laboratories requiring high-throughput analysis. It has been observed that surface coatings on LDTD microwell plates can improve the sensitivity of the analysis of small polar molecules. The objective of the present study is to understand and quantify the effect of microwell surface coatings on signal intensity of small organic molecules of clinical, environmental and forensic interest. Experiments showed that the peak areas of diclofenac, chloramphenicol, salicylic acid and 11-nor-9-carboxy-Δ9-tetrahydrocannabinol obtained by LDTD-QqQMS increased by up to 3 orders of magnitude when using microwells coated with ethylenediaminetetraacetic acid (EDTA). Tests with different chelating agents and polytetrafluoroethylene as microwell surface coatings showed that nitrilotriacetic acid gave significantly higher peak areas for five out of the nine compounds that showed signal enhancement using chelating agents as coatings. Scanning electron microscopy studies of EDTA-coated and uncoated microwells showed that analytes deposited in the former formed more uniform and thinner films than in the latter. The enhancement effect of surface coatings in LDTD-QqQMS was explained mainly by the formation of homogenous and thinner layers of nanocrystals of analytes that are easier to desorb thermally than the layers formed when the analytes dry in direct contact with the bare stainless steel surface. Chemisorption of some analytes to the stainless steel surface of the microwell plate appeared to be a minor factor. Surface coatings widen the number of compounds analyzable by LDTD-QqQMS and can also improve sensitivity and limits of detection.
关键词： pharmaceuticals,high-throughput,hormones,pesticides,x-ray photoelectron spectroscopy,scanning electron microscopy,stainless steel,small organic molecules,chelating agents
更新于2025-09-23 15:23:52
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Formation of Stainless Steel Nanoballs via Submerged Glow-discharge Plasma and their Microstructural Analysis with Evaluation of Photocatalytic Activity
摘要： Stainless steel has shown potential as a catalytic material in bulk form. However, it only becomes active in an aqueous acidic environment and elevated temperatures. This study aims to produce stainless steel nanoparticles that have high photocatalytic activity in a neutral medium and at room temperature and to elucidate the photocatalytic activity mechanism of the nanoparticles. Spherical, photocatalytic nanoparticles called 'nanoballs' were synthesized by the submerged glow-discharge method. Stainless steel SUS316L grade wire was used as the cathode, platinum mesh was used as the anode while the electrolyte was potassium carbonate. The nanoballs were obtained after centrifuging and washing with water. The physical characteristics of the photocatalytic nanoballs were analysed by scanning electron microscopy, high-resolution transmission electron microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction. The nanoballs were mixed with methylene blue and irradiated with ultraviolet light for the evaluation of photocatalytic reaction. The photodecomposition samples were determined using UV-vis spectrometry. The by-products of the photodecomposition were evaluated using mass spectrometry. The results show that stainless steel nanoballs have photocatalytic activity when irradiated with ultraviolet light at room temperature. Submerged glow-discharge plasma method can synthesize nanoparticles rapidly using only metal wires as the electrode.
关键词： photocatalysis,nanoballs,stainless steel,plasma discharge,nanoparticles
更新于2025-09-23 15:22:29
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Effects of LNO buffer layers on electrical properties of BFO-PT thin films on stainless steel substrates
摘要： Ferroelectric 0.7BiFeO3-0.3PbTiO3 (BFO-PT) thin films were deposited on LaNiO3 (LNO) coated stainless steel (SS) substrates by the sol-gel method. XRD results indicate that both LNO and BFO-PT thin films have the perovskite structure and the film crystallinity is improved with increasing the LNO thickness. The dielectric loss of BFO-PT thin films is reduced significantly with addition of LNO buffer layers, achieving about 4 % at the frequency of 1 kHz, much lower than that of > 20 % for BFO-PT thin films directly deposited on SS substrates. BFO-PT thin films reveal the strong ferroelectricity with remnant polarization (Pr) of about 35 m C/cm2 for LNO of 390 nm. Moreover, addition of LNO buffer layers mitigates the polarization deterioration after the 1.33×108 switching cycles resulting in the improved anti-fatigue properties of BFO-PT thin films. Our results indicate that BFO-PT/LNO multilayer thin films on SS substrates maintain excellent dielectric and ferroelectric properties.
关键词： 0.7BiFeO3-0.3PbTiO3 thin films,Stainless steel substrates,LaNiO3
更新于2025-09-23 15:22:29
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Microstructures and Mechanical Properties of Dissimilar Al/Steel Butt Joints Produced by Autogenous Laser Keyhole Welding
摘要： Dissimilar Al/steel butt joints of 6.0 mm thick plates have been achieved using fiber laser keyhole welding autogenously. The cross sections, interface microstructures, hardness and tensile properties of Al/steel butt joints obtained under different travel speeds and laser beam offsets were investigated. The phase morphology and thickness of the intermetallic compound (IMC) layers at the interface were analyzed by scanning electronic microscopes (SEM) using the energy-dispersive spectrometry (EDS) and electron back-scattered diffraction (EBSD) techniques. The results show that travel speeds and laser beam offsets are of considerable importance for the weld shape, morphology and thickness of IMC layers, and ultimate tensile strength (UTS) of Al/steel butt joints. This proves that the IMC layers consist of Fe2Al5 phases and Fe4Al13 phases by EBSD phase mapping. Increasing laser beam offsets from 0.3 mm to 0.7 mm significantly decreases the quantity of Fe4Al13 phases and the thickness of Fe2Al5 layers at the interface. During tensile processing, the Fe2Al5 layer with the weakest bonding strength is the most brittle region at the interface. However, an intergranular fracture that occurred at Fe2Al5 layers leads to a relatively high UTS of Al/steel butt joints.
关键词： laser keyhole welding,IMC layers,Al/steel joints,tensile properties,EBSD phase mapping
更新于2025-09-23 15:21:21