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- PIN diode
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- Ufa State Aviation Technical University
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FFT analysis of surface structures fabricated by laser interference lithography
摘要： This paper presents an FFT (fast Fourier transform) analytical method for the study of surface structures fabricated by laser interference lithography (LIL). In the work, the FFT analytical method combined with Gaussian fitting is used to determine the periods and pattern distributions of surface structures from frequency spectra. For LIL, the processing parameters of incident and azimuth angles can be obtained corresponding to the period and pattern distribution. This work facilitates the detection of micro- and nano-structures, the analysis of pattern distribution in engineering, and the processing error analysis of LIL.
关键词： surface structures,micro- and nano-structures,pattern distribution,laser interference lithography,FFT analysis
更新于2025-11-25 10:30:42
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Surface plasmon resonance of naked gold nanoparticles for photodynamic inactivation of Escherichia coli
摘要： Although antimicrobial photothermal inactivation of naked gold nanostructures using powerful pulsed lasers has been previously studied, there are little reports about their photodynamic antimicrobial properties under the irradiation of low-power density continuous wave lasers. Therefore, this paper attempts to fill this gap. In this paper, we studied the effects of a 40-mW/cm2 continuous Nd:Yag laser at 532 nm and naked gold nanoparticles on inactivation of Escherichia coli ATCC25922. According to our results, 60 min illumination using the Nd:Yag laser caused a 0.15log reduction of the bacterial viability. Also, the employed gold nanoparticles with an average size of 15 nm were toxic to E. coli ATCC 25922 in the concentrations above 0.5 μg/ml. In addition, synergistic effects of 0.5 μg/ml gold nanoparticles and the light illumination led to a 2.43log reduction of the viability after a 60-min exposure and did not show any considerable temperature change on the media. The obtained results were justified based on the possible interaction mechanisms of low-power density laser lights and naked gold nanoparticles. The paper is proposed as a prelude for future research about localized inactivation of resistant pathogens with minimum side effects on neighbor tissues.
关键词： Photodynamic inactivation,Gold nanoparticles,Low-power density laser,Surface plasmon resonance
更新于2025-11-25 10:30:42
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Monolithic metal dimer-on-film structure: new plasmonic properties introduced by the underlying metal
摘要： Dimers -two closely-spaced metallic nanostructures- are one of the primary nanoscale geometries in plasmonics, supporting high local field enhancements in their interparticle junction under excitation of their hybridized “bonding” plasmon. However, when a dimer is fabricated on a metallic substrate, its characteristics are changed profoundly. Here we examine the properties of an Au dimer on an Au substrate. This structure supports a bright “bonding” dimer plasmon, screened by the metal, and a lower energy magnetic charge transfer plasmon. Changing the dielectric environment of the dimer-on-film structure reveals a broad family of higher-order hybrid plasmons in the visible region of the spectrum. Both the localized surface plasmons resonances (LSPR) of the individual dimer-on-film structures as well as their collective surface lattice resonances (SLR) show a highly sensitive refractive index sensing response. Implementation of such all-metal magnetic-resonant nanostructures offers a promising route to achieve higher-performance LSPR- and SLR-based plasmonic sensors.
关键词： Plasmonics,localized surface plasmon resonance,surface lattice resonance,LSPR sensing,refractive index sensing
更新于2025-11-21 11:24:58
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Dielectrophoretic cell trapping for improved surface plasmon resonance imaging sensing
摘要： The performance of conventional surface plasmon resonance (SPR) biosensors can be limited by the diffusion of the target analyte to the sensor surface. This work presents an SPR biosensor that incorporates an active mass-transport mechanism based on dielectrophoresis (DEP) and electroosmotic flow to enhance analyte transport to the sensor surface and reduce the time required for detection. Both these phenomena rely on the generation of AC electric fields that can be tailored by shaping the electrodes that also serve as the SPR sensing areas. Numerical simulations of electric field distribution and microparticle trajectories were performed to choose an optimal electrode design. The proposed design improves on previous work combining SPR with DEP by using face-to-face electrodes, rather than a planar interdigitated design. Two different top-bottom electrode designs were experimentally tested to concentrate firstly latex beads and secondly biological cells onto the SPR sensing area. SPR measurements were then performed by varying the target concentrations. The electrohydrodynamic flow enabled efficient concentration of small objects (3 μm beads, yeasts) onto the SPR sensing area, which resulted in an order of magnitude increased SPR response. Negative dielectrophoresis was also used to concentrate HEK293 cells onto the metal electrodes surrounded by insulating areas, where the SPR response was improved by one order of magnitude.
关键词： dielectrophoresis,electro-osmosis,biosensing instrumentation,top-bottom electrodes,surface plasmon resonance
更新于2025-11-21 11:24:58
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Determination of nanoscale titanium oxide thin film phase composition using X-ray photoelectron spectroscopy valence band analysis
摘要： The phase compositions of nanoscale thick titania films on the titanium were determined using X-ray photoelectron spectroscopy valence band analysis for the first time, by deconvoluting the two-peak structure of valence band into five peaks and analysing the relative peak area. The titania films of thickness varying from about 2 nm to 8 μm were obtained by the air oxidation of commercially pure titanium at different temperatures. The titania films formed on titanium for oxidizing temperatures up to 200 °C were amorphous, with thickness < 10 nm. The sub-stoichiometric oxides present at the TiO2-Ti interface were composed of Ti3+, Ti2+ and Ti1+ states when the film of thickness was < 10 nm. At 300 °C, when the titania film thickness was < 20 nm, it was fully converted to rutile phase and remained stable up to 1000 °C. A broadening of full-width half-maxima of the core level peaks for the titania layers was attributed to the presence of surface hydroxyl group and stress gradient within the oxide layer. The absence of metastable anatase phase in the titania layers at lower temperatures was attributed to the presence of high stresses within the oxide layers owing to their nanoscale thickness.
关键词： X-ray Photoelectron Spectroscopy,Thin film,Valence band,Surface phase composition,Titania,Titanium
更新于2025-11-21 11:24:58
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Surface Coatings Modulate the Differences in the Adhesion Forces of Eukaryotic and Prokaryotic Cells as Detected by Single Cell Force Microscopy
摘要： Single cell force microscopy was used to investigate the maximum detachment force (MDF) of primary neuronal mouse cells (PNCs), osteoblastic cells (MC3T3), and prokaryotic cells (Staphylococcus capitis subsp. capitis) from different surfaces after contact times of 1 to 5 seconds. Positively charged silicon nitride surfaces were coated with positively charged polyethyleneimine (PEI) or poly-D-lysine. Laminin was used as the second coating. PEI induced MDFs of the order of 5 to 20 nN, slightly higher than silicon nitride did. Lower MDFs (1 to 5 nN) were detected on PEI/laminin with the lowest on PDL/laminin. To abstract from the individual cell properties, such as size, and to obtain cell type-specific MDFs, the MDFs of each cell on the different coatings were normalized to the silicon nitride reference for the longest contact time. The differences in MDF between prokaryotic and eukaryotic cells were generally of similar dimensions, except on PDL/laminin, which discriminated against the prokaryotic cells. We explain the lower MDFs on laminin by the spatial prevention of the electrostatic cell adhesion to the underlying polymers. However, PEI can form long flexible loops protruding from the surface-bound layer that may span the laminin layer and easily bind to cellular surfaces and the small prokaryotic cells. This was reflected in increased MDFs after two-second contact times on silicon nitride, whereas the two-second values were already observed after one second on PEI or PEI/laminin. We assume that the electrostatic charge interaction with the PEI loops is more important for the initial adhesion of the smaller prokaryotic cells than for eukaryotic cells.
关键词： prokaryotic cells,poly-D-lysine,silicon nitride,laminin,cell adhesion,single cell force microscopy,surface coatings,polyethyleneimine,eukaryotic cells,maximum detachment force
更新于2025-11-21 11:24:58
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Surface nanocrystallization of Cu-Cr alloy by a high power density continuous laser beam
摘要： A nanostructured surface layer of (cid:1)300 lm thickness was fabricated on Cu-30Cr (wt%) hypereutectic alloy by a continuous laser beam with high power density (1.08 (cid:3) 107 W/cm2). The average grain size of Cr-rich particles was re?ned to (cid:1)40 nm, and the solid solubility limit of Cr in Cu was extended to 1.96 at. %. Experimental results show that the dispersion of nano-sized Cr-rich spheroids in Cu-rich matrix was attributed to the Brownian motion of Cr-rich spheroids, and the high cooling rate (5.75 (cid:3) 106 K/s) during liquid phase separation which inhibits the collisions between Cr-rich spheroids.
关键词： Solidi?cation,Surface nanocrystallization,Microstructure,Cu-Cr alloy,Laser surface melting
更新于2025-11-21 11:18:25
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Possibilities of Dry and Lubricated Friction Modification Enabled by Different Ultrashort Laser-Based Surface Structuring Methods
摘要： In this contribution we report on the possibilities of dry and lubricated friction modification introduced by different laser surface texturing methods. We compare the potential of Laser-Induced Periodic Surface Structures and Laser Beam Interference Ablation on 100Cr6 steel in a linear reciprocating ball-on-disc configuration using 100Cr6 steel and tungsten carbide balls with load forces between 50 mN and 1000 mN. For dry friction, we find a possibility to reduce the coefficient of friction and we observe a pronounced direction dependency for surfaces fabricated by Laser Beam Interference Ablation. Furthermore, Laser-Induced Periodic Surface Structures result in a load-dependent friction reduction for lubricated linear reciprocating movements. This work helps to identify the modification behaviour of laser generated micro structures with feature sizes of approximately 1 μm and reveals new possibilities for surface engineering
关键词： lubricated friction,smart surfaces,laser surface texturing,laser beam interference ablation,laser-induced periodic surface structures,dry friction
更新于2025-11-21 11:18:25
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A study of metallurgy and erosion in laser surface alloying of AlxCu0.5FeNiTi high entropy alloy
摘要： AlxCu0.5FeNiTi high entropy alloy coating is synthesized by premixed high purity Cu, Fe, Ni and Ti powders on AA1050 aluminium substrate by laser surface alloying, with the aim to improve microhardness and erosion rate. Phase constituents, microstructure and microhardness were investigated using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and Vickers Microhardness tester, respectively. The erosion behavior of AlxCu0.5FeNiTi coating is checked using an air jet erosion setup. SEM images show presence of three regions. Percentage compositions of these regions are evaluated using Energy Dispersive Spectroscopy. XRD analysis of AlxCu0.5FeNiTi coating confirmed that these regions are a mixture of disordered BCC and two FCC solid solution phases. The microhardness of the AlxCu0.5FeNiTi HEA is 18 times that of the AA1050 aluminium substrate. Results show that AlxCu0.5FeNiTi HEA coating has improved erosion resistance.
关键词： Laser Surface Alloying,Microhardness,Microstructure,High Entropy Alloy,Erosion rate
更新于2025-11-21 11:18:25
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Conductive treatment of Piezoelectric Composite Material by low-temperature adhesion comparing with ion sputtering
摘要： The surface conductive treatment is an essential step for piezoelectric composite material being application, but until now there are many issues remain to be solved. A conductive adhesion with low curable temperature, low resistivity and high welding spot adhesion strength was obtained for the conductive treatment of piezoelectric composite material. The welding spot adhesion strength was defined at first time. The conductive and adhesion properties were studied comparing with samples treated by ion sputtering. The conductive adhesive with curing agent of EDA has the lowest resistivity of 1.973× 10-4 Ω·cm and the highest welding spot adhesion strength of 7.93MPa.
关键词： Surface conductive treatment,Silver compounds,Adhesive,Piezoelectric Composites
更新于2025-11-21 11:18:25