研究目的
Investigating the microstructural evolution during 3D laser printing of Ti-6Al-4V using operando X-ray diffraction to understand the influence of laser and scanning parameters on phase transformations, heating and cooling rates, and residual stress formation.
研究成果
The MiniSLM device combined with high-flux synchrotron X-ray diffraction allows for detailed observation of microstructural evolution during 3D laser printing. The scanning strategy significantly influences the thermal history and resulting microstructure, with shorter scanning vectors leading to longer durations in the high-temperature phase and different microstructural features. This insight is crucial for optimizing printing parameters to achieve desired material properties.
研究不足
The study is limited to Ti-6Al-4V alloy and may not be directly applicable to other materials. The operando measurements provide averaged information over the volume probed by the X-ray beam, which may not capture local variations. The experiments are performed at a synchrotron facility, limiting accessibility for routine industrial applications.
1:Experimental Design and Method Selection:
The study uses a newly developed in operando X-ray diffraction device at a synchrotron beamline to perform real-time measurements during laser 3D printing. The methodology includes tracking the temporal evolution of phases, measuring heating and cooling rates, and observing residual stress formation.
2:Sample Selection and Data Sources:
Ti-6Al-4V commercial alloy powder is used for printing. The powder characteristics and chemical composition are analyzed using SEM and EDS.
3:List of Experimental Equipment and Materials:
The setup includes a miniaturized SLM device (MiniSLM), a 500 W redPOWER continuous wave Fiber Laser, a 2-axis deflection-scanning unit, and an EIGER detector for X-ray diffraction.
4:Experimental Procedures and Operational Workflow:
The experiments involve printing with different laser powers and scanning strategies while recording diffraction patterns at high frame rates to capture the phase evolution and thermal history.
5:Data Analysis Methods:
The diffraction data is analyzed to determine phase fractions, temperatures, and cooling rates. EBSD is used for microstructure analysis.
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