研究目的
Investigating the development and characterization of TiNiCu shape memory alloy structures using laser additive manufacturing.
研究成果
The LAM process was successful in developing TiNiCu bulk SMA structures. TiNiCu10 showed the best properties among the developed samples. The study provides a foundation for further research on microstructure engineering to improve TiNiCu20 and TiNiCu30 samples.
研究不足
The study focused on three specific compositions of TiNiCu and used a specific LAM system. The results may vary with different compositions or manufacturing techniques.
1:Experimental Design and Method Selection:
The study involved the development of TiNiCu shape memory alloys using laser additive manufacturing (LAM) and numerical simulation to predict residual stress flow.
2:Sample Selection and Data Sources:
Three different compositions of TiNiCu (Ti50Ni (50?x) Cux (x = 10, 20 and 30)) were used.
3:List of Experimental Equipment and Materials:
A 2 kW fiber laser, pre mixed powders of Ti, Ni, and Cu, SEM, AFM, micro-hardness tester, compression test machine, XRD, and DSC were used.
4:Experimental Procedures and Operational Workflow:
The deposition process was simulated using FEM with Gaussian distributed volumetric heat source. The developed samples were characterized for surface morphology, mechanical properties, crystalline nature, and phase transformation ability.
5:Data Analysis Methods:
The data was analyzed using SEM, AFM, micro-hardness test, compression test, XRD, and DSC.
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SEM
Supra55
Zeiss
Study the surface morphology of the samples
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AFM
NSE
Nanoscope-E
Nanometric level surface analyses
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XRD
Smart Lab Automated Multipurpose
Rigaku
Investigate the crystalline nature of the samples
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fiber laser
2 kW
Heat source for melting the pre mixed powders of Ti, Ni, and Cu
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micro-hardness tester
VMH 002
UHL
Analyze the mechanical properties of the samples
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compression test machine
Makron UTS-02-0010
Biss
Analyze the mechanical properties of the samples
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DSC
DSC 214
Netzsch
Study the phase transformation property
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