研究目的
Investigating the fabrication and electroluminescence properties of sheet-like ZnO/Si light-emitting diodes using a radio frequency magnetron sputtering method.
研究成果
The fabrication conditions significantly affect the structures and EL spectra of ZnO/Si LEDs. Understanding these conditions is crucial for the purposeful application of sheet-like ZnO by RF magnetron sputtering method.
研究不足
The study highlights the sensitivity of structures and EL properties to fabrication conditions, suggesting the need for optimization in future works.
1:Experimental Design and Method Selection:
The study employed a radio frequency (RF) magnetron sputtering method to deposit nanoscale ZnO on p-type single crystal silicon.
2:Sample Selection and Data Sources:
p-type crystal silicon with (111) orientation and a resistivity of
3:007~008 cm·Ω was used. List of Experimental Equipment and Materials:
JPG-560 magnetron sputtering deposition system, ZnO target with purity of
4:99%, ITO and Ag electrodes. Experimental Procedures and Operational Workflow:
The sputtering chamber was pumped to less than 10-5 Pa before deposition, argon gas was used to maintain constant pressure, and depositions were carried out at 300 oC.
5:Data Analysis Methods:
XRD, FESEM, HR-TEM, UV-vis-NIR spectrophotometer, and spectrofluorometer were used for characterization.
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UV-vis-NIR spectrophotometer
UV-3150
Shimadzu
Obtaining absorption spectra.
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Double grating spectrofluorometer
FL3-22
HORIBA
Collecting EL spectra.
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JPG-560 magnetron sputtering deposition system
JPG-560
Chinese Academy of Sciences, Shenyang Scientific Instrument Co., Ltd.
Used for depositing nanoscale ZnO on p-type crystal silicon.
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Field emission scanning electron microscopy
JSM 6700F
Characterization of morphological and structural properties.
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High-resolution transmission electron microscope
JEM-2100
Characterization of morphological and structural properties.
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X-ray diffraction
Panalytical X’Pert Pro
Characterization of structural properties.
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