研究目的
To study the effect of high-power, high-brightness disk laser welding on the microstructure evolution of PM Ti-51 at.% Ni welds, and elucidate its correlation with mechanical properties and superelasticity.
研究成果
High-power high-brightness laser welding successfully joined fully dense SPS-processed Ti-51 at.% Ni SMAs, producing sound welds with some microporosities. The microstructure of the welds was significantly altered, with coarse columnar grains in the fusion zone. Optimal welding parameters were found to be a laser power of 3 kW and welding speed of 6 m/min.
研究不足
The presence of microporosity imperfections in the welds and the need for post-weld heat treatment to induce Ti3Ni4 precipitations again.
1:Experimental Design and Method Selection:
Utilized a high-power, high-brightness disk laser welding process to join spark-plasma-sintered Ti-51 at.% Ni shape memory alloy.
2:Sample Selection and Data Sources:
Commercially pure powders of Ti and Ni were used to produce PM Ti-51 at.% Ni SMA.
3:List of Experimental Equipment and Materials:
High-power, high-brightness continuous wave disk laser (TRUMPF-TruDisk 16002), spark plasma sintering system (SPS-1030S, SPS Syntex), hydraulic pressing machine (SHP-200-450, Shibayama), field emission scanning electron microscope (JEM-6500F, JEOL), transmission electron microscope (JEM-2100F, JEOL), x-ray diffractometer (XRD-6100, Shimadzu), micro-XRD system (XRD, Bruker-D8).
4:8). Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: Samples were cut using wire cut electrical discharge machining, welded using laser welding, and then subjected to microstructural characterization.
5:Data Analysis Methods:
Microstructural observations were carried out using SEM, TEM, XRD, and EBSD.
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Field emission scanning electron microscope
JEM-6500F
JEOL
Used for high-resolution imaging and elemental scanning.
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Transmission electron microscope
JEM-2100F
JEOL
Used for high-resolution imaging and elemental scanning.
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X-ray diffractometer
XRD-6100
Shimadzu
Used for phase identification of the base metal and welds.
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Micro-XRD system
XRD, Bruker-D8
Bruker
Used for phase identification of the base metal and welds.
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High-power, high-brightness continuous wave disk laser
TRUMPF-TruDisk 16002
TRUMPF
Used for laser welding of the Ti-51 at.% Ni shape memory alloy.
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Spark plasma sintering system
SPS-1030S
SPS Syntex
Used for consolidating commercially pure powders of Ti and Ni to produce PM Ti-51 at.% Ni SMA.
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Hydraulic pressing machine
SHP-200-450
Shibayama
Used for hot forging process to obtain 50% of height reduction.
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