研究目的
Investigating the influence of fabrication methods on the optical and photo-thermal properties of nano-LaB6.
研究成果
The study successfully demonstrated the fabrication of nano-LaB6 particles using ball milling and plasma technology, highlighting the superior properties of plasma-synthesized NPs. It also established methods for stabilizing these NPs and characterized their photo-thermal conversion properties, suggesting potential applications in areas requiring controlled optical and thermal properties.
研究不足
The study notes the contamination of LaB6 by ZrO2 grinding media in milling experiments and the need for stabilization of NPs in dispersion media to prevent agglomeration and sedimentation.
1:Experimental Design and Method Selection:
The study compares two fabrication methods for nano-LaB6: continuously operated ball milling and induction plasma technology.
2:Sample Selection and Data Sources:
Nano particles (NPs) were manufactured using ethylene glycol (EG) and ZrO2 grinding media.
3:List of Experimental Equipment and Materials:
Equipment includes a continuously operated laboratory mill MiniSerie from Netzsch, ZrO2 grinding media, and various dispersion media (ethanol, 1-methoxy-2-propanol, ethylene glycol).
4:Experimental Procedures and Operational Workflow:
Grinding experiments were performed under various parameters, and the properties of the resulting NPs were characterized using techniques like Dynamic Light Scattering, UHR-FESEM, and X-Ray diffraction.
5:Data Analysis Methods:
The absorption behavior and photo-thermal conversion properties of the NPs were analyzed, and the temperature distribution around the laser spot was characterized by an IR camera.
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