研究目的
Investigating the effect of ultrashort pulsed laser texturing on the microstructure and properties of metastable S phase layer formed on AISI 316L surfaces.
研究成果
The study demonstrated that femtosecond laser texturing is feasible for S phase treated surfaces without causing decomposition or loss of corrosion resistance, paving the way for long-lasting multi-functional antibacterial stainless steel surfaces. Nanosecond laser texturing, however, led to damage and decomposition of the S phase.
研究不足
The study is limited to the effects of ultrashort pulsed laser texturing on S phase treated AISI 316L surfaces. The thermal nature of laser texturing and the metastability of the S phase pose challenges for combining these technologies without detrimental effects.
1:Experimental Design and Method Selection:
The study involved active screen plasma nitriding (ASPN) of AISI 316L austenitic stainless steel samples followed by laser texturing using femtosecond and nanosecond pulsed lasers. The response of the S phase treated surfaces to laser texturing was investigated through surface characterization, electrochemical corrosion testing, and temperature modelling.
2:Sample Selection and Data Sources:
AISI 316L austenitic stainless steel cylinders were used. The samples were ground, polished, and cleaned before ASPN treatment.
3:List of Experimental Equipment and Materials:
Equipment included a DC Kl?ckner Ionon 40 kW plasma furnace for ASPN, MOPA-based Yb-doped fibre and Satsuma from Amplitude Systemes for laser texturing, GDOES for elemental depth profiling, Vicker’s microhardness tester, Raman microscope, XRD, SEM, TEM, and electrochemical testing instruments.
4:Experimental Procedures and Operational Workflow:
Samples were treated with ASPN, then textured with lasers under different settings. Surface characterization and electrochemical tests were performed to assess the effects.
5:Data Analysis Methods:
Data from GDOES, hardness tests, Raman spectroscopy, XRD, SEM, TEM, and electrochemical tests were analyzed to evaluate the microstructure, properties, and corrosion resistance of the textured surfaces.
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JEOL 7000F
7000F
JEOL
Scanning electron microscopy for examining surface morphology.
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FEI Quanta 3D
Quanta 3D
FEI
Focussed ion beam milling for TEM sample preparation.
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JEOL 2100 TEM
2100
JEOL
Transmission electron microscopy for studying surface microstructure.
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Bruker D8 Advanced
D8 Advanced
Bruker
X-ray diffraction using a Cu radiation source.
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GDA 650 Spectruma Analytic Gmbh
GDA 650
Spectruma Analytic Gmbh
Glow-discharge optical emission spectrometer for elemental depth profiling.
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Mitutoyo MVK-H1 Vicker’s microhardness tester
MVK-H1
Mitutoyo
Measuring surface hardness with a load of 50 gram-force (gf).
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Renishaw inVia Raman Microscope
inVia
Renishaw
Raman spectroscopy with a 488 nm excitation laser.
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Gammry Interface 1000
Interface 1000
Gammry
Electrochemical corrosion testing instrument.
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