研究目的
To develop a simple one-step recycling method for converting discharged batteries, a major constituent of electronic waste (e-waste), into value-added fluorescent nanomaterials-carbon quantum dots (CQDs) and plasmonic nanostructures (eW-Au@CQDs) for surface-enhanced Raman scattering (SERS) applications.
研究成果
The study successfully demonstrated the conversion of e-waste into value-added nanomaterials with potential applications in SERS-based sensing. The eW-Au@CQDs showed promising results for the detection of MB, indicating their potential for environmental and bioanalytical applications.
研究不足
The study primarily focuses on the synthesis and preliminary application of eW-CQDs and eW-Au@CQDs for SERS. Further optimization is needed for their practical application in environmental and bioanalysis.
1:Experimental Design and Method Selection
The study involved the synthesis of eW-CQDs from discharged Duracell AA batteries through high-temperature pyrolysis and their use as reducing/capping agents for the synthesis of eW-Au@CQDs. The optical, morphological, and structural properties of these nanomaterials were characterized using various techniques.
2:Sample Selection and Data Sources
Carbon additives from discharged Duracell AA batteries were used as the source material for synthesizing eW-CQDs.
3:List of Experimental Equipment and Materials
Discharged Duracell AA batteries, hydrogen tetrachloroaurate (HAuCl4), hydrochloric acid (HCl), sulfuric acid (H2SO4), sodium chloride (NaCl), methylene blue (MB), ethanol, acetone, dialysis membrane, syringe filters, centrifuge, UV–visible spectrophotometer, spectro-fluorimeter, Raman spectrometer, transmission electron microscope, X-ray diffractometer.
4:Experimental Procedures and Operational Workflow
The synthesis involved pyrolysis of carbon additives at 220°C for 30 minutes, followed by purification. eW-Au@CQDs were synthesized by mixing eW-CQDs with HAuCl4. The nanomaterials were characterized and tested for SERS applications using MB as a model dye.
5:Data Analysis Methods
Optical properties were analyzed using UV–visible absorption and photoluminescence spectroscopy. Morphological and structural properties were determined using HRTEM, SAED, and XRD. SERS signals were recorded and analyzed for MB detection.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容-
Transmission electron microscope
H-7500
Hitachi Ltd.
Particle size and morphological characteristics determination
暂无现货
预约到货通知
-
X-ray diffractometer
PANALYTICAL X’Pert PRO
PANALYTICAL
Crystal structure investigation
暂无现货
预约到货通知
-
CHI 1040A electrochemical workstation
CHI 1040A
CH Instruments
Electrodeposition of gold onto screen-printed carbon electrodes
暂无现货
预约到货通知
-
Ocean Optics QEPro High-Performance Spectrometer
QEPro
Ocean Optics
SERS measurements
暂无现货
预约到货通知
-
Hitachi U-3900-H spectrophotometer
U-3900-H
Hitachi
UV–visible absorption spectra recording
暂无现货
预约到货通知
-
FS5 Edinburgh spectro-fluorimeter
FS5
Edinburgh
Fluorescence properties analysis
-
Duracell AA batteries
Duracell
Source material for carbon quantum dots synthesis
暂无现货
预约到货通知
-
inVia instrument, Renishaw
inVia
Renishaw
Raman spectroscopy
暂无现货
预约到货通知
-
登录查看剩余6件设备及参数对照表
查看全部