研究目的
Investigating the effect of increasing sample temperature and cavity confinement sizes on the emission intensities and plasma dynamics of laser-induced magnesium (Mg) and titanium (Ti) plasmas.
研究成果
Increasing sample temperature significantly enhances plasma emission intensities and affects plasma dynamics. Smaller cavity sizes improve emission intensities and electron temperatures due to plasma compression effects. The findings suggest potential for optimizing LIBS applications through temperature control and cavity confinement.
研究不足
The study is limited to Mg and Ti alloys under specific laser and environmental conditions. The effects of other materials or different ambient conditions were not explored.
1:Experimental Design and Method Selection:
A Q-switched Nd:YAG laser system operating at 1064 nm was used to generate plasmas on Mg and Ti alloy samples. The effect of sample temperature and cavity confinement sizes on plasma emission intensities and dynamics was studied.
2:Sample Selection and Data Sources:
Titanium and magnesium alloys with high purity were used. Emission spectra were collected using an echelle spectrometer with an ICCD camera.
3:List of Experimental Equipment and Materials:
Nd:YAG laser, echelle spectrometer, ICCD camera, delay generator, digital oscilloscope, heating element with thermocouple, circular and square cavities.
4:Experimental Procedures and Operational Workflow:
The laser was focused on the sample surface to generate plasma. The emitted light was collected and analyzed. Sample temperature was varied, and different cavity sizes were used to confine the plasma.
5:Data Analysis Methods:
Emission intensities were analyzed using Boltzmann and Saha–Boltzmann plots for electron temperature and Stark broadening for electron density.
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ICCD camera
iStar DH-334T
Andor Technology
Capturing plasma emission
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Delay generator
DG645
Stanford Research System
Synchronizing laser pulses and ICCD
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Digital oscilloscope
DL9140
YOKOGAWA
Monitoring signals
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Echelle spectrometer
Mechelle 5000
Andor Tech.
Analyzing emitted plasma radiation
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Nd:YAG laser
Q-switched
Generating plasma on sample surfaces
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