研究目的
To determine the effects of cold rolling, recrystallization and laser surface melting (LSM) on the microstructure and mechanical properties of a biphase (α″+β) Ti?30Nb?4Sn alloy.
研究成果
LSM of the deformed alloy produced changes in hardness, elastic modulus, and crystallographic texture similar to those produced by recrystallization heat treatment, creating a stiffness gradient between surface and substrate. The study highlights the potential of LSM as an alternative method for changing the surface properties of alloys, such as corrosion resistance and biocompatibility.
研究不足
The β-phase texture could not be directly measured by XRD due to peak overlapping with α″ peaks. The study suggests further research to determine the effects of surface?substrate stiffness gradients on the biomechanical behavior of implants.
1:Experimental Design and Method Selection:
The study involved cold rolling, recrystallization, and laser surface melting (LSM) treatments on Ti?30Nb?4Sn alloy to analyze their effects on microstructure and mechanical properties.
2:Sample Selection and Data Sources:
The alloy was produced in an electric arc furnace, homogenized, water quenched, and cold-rolled to an 85% reduction in thickness. Part of the rolled sample was heat-treated for recrystallization.
3:List of Experimental Equipment and Materials:
Equipment included an X-ray diffractometer (Panalytical X’Pert Pro), nanoindenter (G?200 from Agilent Technology), and electron microscope (ZEISS AURIGA Compact).
4:Experimental Procedures and Operational Workflow:
The alloy underwent cold rolling, recrystallization heat treatment, and LSM. Microstructure and texture were analyzed using XRD and EBSD. Hardness and elastic modulus were measured using nanoindentation.
5:Data Analysis Methods:
Texture analysis was performed using the MTEX toolbox for MATLABTM. Nanoindentation data were analyzed to determine hardness and elastic modulus.
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