研究目的
To investigate the mechanical properties of Young’s modulus and fatigue of aluminum nitride films deposited on 304 stainless steel foils for reliable design of piezoelectric vibration energy harvesters.
研究成果
The Young’s modulus of SUS 304 foil and sputtered AlN film was measured to be 184.9 and 342.9 MPa, respectively. The fatigue strength of SUS 304 foils and the material with AlN/ SUS 304/ AlN structure was estimated to be 294 and 327 MPa, respectively. Fatigue failures were observed on SUS 304 foils but not on AlN films. The study suggests designing AlN-based PVEHs to work at stresses below the fatigue strength of 327 MPa for long-term reliability.
研究不足
The study focused on specific thicknesses of SUS 304 foils and AlN films. The fatigue behavior of sputtered AlN films was not compared with other deposition methods or materials. The influence of environmental factors on fatigue properties was not considered.
1:Experimental Design and Method Selection:
The study involved micro-fabricating cantilevers from SUS 304 foils and AlN films deposited on SUS 304 foils. Young’s modulus was measured using the micro-cantilever resonance method, and fatigue properties were investigated using the resonant bending fatigue testing method.
2:Sample Selection and Data Sources:
SUS 304 foils with a thickness of 50 μm and a composite material of AlN films deposited on both sides of SUS 304 foils were used. The samples were micro-fabricated to cantilevers.
3:List of Experimental Equipment and Materials:
Equipment included a signal generator with a shaker, a pair of positioning fixtures, a laser displacement sensor with a controller, an oscilloscope, and a controlling personal computer. Materials included SUS 304 foils, AlN films, Cr and Au films, and Cu proof mass.
4:Experimental Procedures and Operational Workflow:
The samples were subjected to resonant frequency measurements and fatigue tests. The displacement amplitude was recorded, and FE analysis was performed to calculate the stress of the cantilevers.
5:Data Analysis Methods:
The Young’s modulus was calculated from the resonant frequency. Fatigue life was determined by the change in amplitude versus number of cycles. Stress-cycle (S-N) curves were plotted to analyze fatigue properties.
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