研究目的
The objective is focusing on the reaction synthesis that fabricates the self-lubricating composite coating that contains solid-lubricant phase CrS, as well as exploring the idea that ceramic particles contribute to improving the microstructural evolution of the coating. Besides, the tribological behavior of the coatings was also explored.
研究成果
Co-based metal matrix self-lubricating coatings containing solid-lubricant phase CrS and ceramic reinforced phase NbC were successfully fabricated. NbC plays a key role in improving CrS nuclear and refining microstructure. The coatings showed improved microhardness and tribological properties, with coating 4 exhibiting the best performance.
研究不足
The study does not consider the effect of ceramic particles on the formation mechanism of CrS in detail. The comprehensive effect of CrS and ceramic particles on the wear mechanism needs further exploration.
1:Experimental Design and Method Selection
Laser cladding was used to fabricate Co-based self-lubricating composite coatings on Cr12MoV steel surface. The phase composition, microstructure, and tribological properties were investigated using XRD, SEM, EDS, and dry sliding wear testing.
2:Sample Selection and Data Sources
Flat plate of unheated-treated Cr12MoV steel was selected as substrate. Co-based alloy powder (Stellite 6), WS2, and NbC were used as cladding materials.
3:List of Experimental Equipment and Materials
IPG-YLS-5000 fiber laser system, SEM (Hitachi/S-3400), EDS, XRD (PANalytical/X’Pert Pro), Vickers microhardness tester (HXD-1000TMSC/LCD), pin-on-disc friction and wear testing machine (Bruker/UMT-3), optical microscopy (KEYENCE/VHX-5000).
4:Experimental Procedures and Operational Workflow
Mixed powders were preplaced on the substrate without using a binder. Laser cladding was performed with optimized parameters. The coatings were characterized and tested for microhardness and wear resistance.
5:Data Analysis Methods
Microhardness was measured using a Vickers microhardness tester. Wear rate was calculated based on wear volume, load, and sliding distance.
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IPG-YLS-5000 fiber laser system
YLS-5000
IPG
Used for laser cladding process.
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SEM
S-3400
Hitachi
Characterization of microstructure and element distribution.
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XRD
X’Pert Pro
PANalytical
Identification of crystal phases of coatings.
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Pin-on-disc friction and wear testing machine
UMT-3
Bruker
Dry sliding friction test.
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Vickers microhardness tester
HXD-1000TMSC/LCD
Measurement of microhardness along the depth direction of coating.
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Optical microscopy
VHX-5000
KEYENCE
Measurement of wear volumes of the coatings.
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