研究目的
Development of a new material and technology for solar energy collectors capable of withstanding high temperatures in corrosive environments for extended periods.
研究成果
The developed glass-crystalline enamel coating on stainless steel pipes can withstand temperatures ≥ 600 °C for at least 250 days, with high thermal expansion coefficients matching the metal substrate. The addition of a sol-gel coating enhances chemical resistance and maintains original microhardness. Future work will explore hydrophobicity and hydrophilicity of the coatings.
研究不足
The study focuses on temperatures up to 600 °C and does not explore higher temperature ranges. The long-term stability beyond 9000 hours is not verified.
1:Experimental Design and Method Selection:
Development of glass-crystalline enamel coatings adhered to tubular stainless steel pipes with high coefficients of thermal expansion (CTE).
2:Sample Selection and Data Sources:
Use of chromium-nickel stainless steel pipes and various enamel compositions.
3:List of Experimental Equipment and Materials:
X-ray analysis equipment, muffle oven, atomic force microscopy, scanning electron microscopy, UV/VIS spectrophotometer, Vickers hardness tester, thermal radiation thermometer.
4:Experimental Procedures and Operational Workflow:
Preparation of enamel coatings, application of sol-gel coatings, heat treatment, and testing for thermal stability, chemical resistance, and optical properties.
5:Data Analysis Methods:
Analysis of X-ray patterns, reflectance spectra, microhardness, and chemical resistance.
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Rigaku Ultima+
Ultima+
Rigaku
X-ray analysis with CuKα radiation and goniometer rotation
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Veeco SPM II
SPM II
Veeco
Atomic force microscopy using a tapping mode
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Shamidzu SolidSpec-3700
SolidSpec-3700
Shamidzu
UV/VIS spectrophotometer
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Elmer Perkin LAMBDA 650
LAMBDA 650
Elmer Perkin
UV/VIS photospectrometer
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NovaNanoSEM 650
NovaNanoSEM 650
NovaNano
Scanning electron microscopy
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Vickers M41
M41
Vickers
Hardness and elastic modulus examination
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CEM DT-8863
DT-8863
CEM
Infrared thermometer
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Peak Tech 4975
4975
Peak Tech
Thermal radiation thermometer
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KN 4002 KSV NIMA Dip Coater Single Vessel System Small
KN 4002
KSV NIMA
Dip-coating method for film growth
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