研究目的
To examine the photocatalytic effects of ZnO nanoparticles multilayer films on the degradation of organic dyes under ultraviolet light.
研究成果
Zinc oxide nanoparticles and their multilayer films were successfully synthesized and showed effective photocatalytic degradation of organic dyes under ultraviolet light, with methylene blue being the most effectively degraded.
研究不足
The study focuses on the photocatalytic degradation of specific organic dyes under controlled conditions, which may not represent all possible environmental contaminants.
1:Experimental Design and Method Selection:
Synthesis of ZnO nanoparticles under ultrasonic irradiation and preparation of ZnO nanoparticles multilayer films.
2:Sample Selection and Data Sources:
Use of zinc nitrate hexahydrate, sodium hydroxide, and organic dyes (methylene blue, methyl orange, rhodamine B).
3:List of Experimental Equipment and Materials:
Ultrasonic generator, UV lamp, TEM, SEM, XRD, UV-visible spectrophotometer.
4:Experimental Procedures and Operational Workflow:
Synthesis of ZnO nanoparticles, preparation of multilayer films, and evaluation of photocatalytic activity.
5:Data Analysis Methods:
Characterization by TEM, SEM, XRD, and UV-visible spectrophotometry.
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transmission electron microscopy
JEM-2010
JEOL Ltd
Analyzing the morphology and crystallite size of ZnO nanoparticles.
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scanning electron microscopy
JSM-6510
JEOL Ltd
Examining the surface of synthesized ZnO nanoparticles.
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X-ray diffraction
D8 Advance
Bruker
Characterizing the structure of synthesized ZnO nanoparticles.
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UV-visible spectrophotometer
UV-1601 PC
Shimazu
Performing UV-visible spectroscopy of the samples.
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ultrasonic generator
UGI1200
Hanil Ultrasonic Co., Ltd.
Conducting ultrasonic irradiation of all samples.
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UV lamp
77202
Marne La Valee-cedex 1 France
Used as the ultraviolet light irradiation source.
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