研究目的
To understand the mechanism of the direct bonding system between tellurite and silicate glasses at RT with 15% and 62% RH without post-heat treatment.
研究成果
Tellurite glass film was successfully bonded to silicate glass surface at room temperature and moderate or low relative humidity (62% and 15%, respectively). The tellurite thin film adhered more strongly to the silicate glass substrate at 15% RH (adhesive strength ~250 mJ/m2) than at 62% RH. The RH during the bonding process is an important factor of the adhesive strength at the thin-film-substrate interface. The direct bonding technique is much more easily implemented than other procedures in practical operations.
研究不足
The study is limited by the conditions of direct bonding at room temperature without post-heat treatment, and the specific RH conditions tested (15% and 62%). The mechanism might vary under different conditions or with post-heat treatments.
1:Experimental Design and Method Selection:
The study involved the fabrication of tellurite glass thin films using the glass blowing technique and their direct bonding to silicate glass substrates at room temperature under two different relative humidity conditions (15% and 62%).
2:Sample Selection and Data Sources:
Tellurite glass films with thicknesses of 1–3 μm were placed onto silicate glass substrates. The composition of the silicate glass was specified.
3:List of Experimental Equipment and Materials:
Equipment included a gold crucible for melting, a silica glass tube for blowing, nitrogen gas for inflation, and various analytical instruments like SEM, AFM, FT-IR, and TGA.
4:Experimental Procedures and Operational Workflow:
The process involved melting tellurite glass, blowing it into thin films, conditioning at specific RH, bonding to silicate glass, and pressing under approximately 1000 Pa for 2–3 s.
5:Data Analysis Methods:
Adhesive strength was measured using the Obreimoff-Metsik method, and hydroxyl groups were analyzed by FT-IR. Water and OH groups on surfaces were quantified by TGA.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容