研究目的
Investigating the synthesis and characterization of two novel organic?inorganic hybrids using tellurite anions as heteroanion templates and linkers.
研究成果
Two unique polyoxoniobate compounds were isolated and characterized, demonstrating the role of tellurite anions in facilitating the formation of complex architectures. The crystal growth methods were crucial for the formation of aggregations, suggesting avenues for future exploration of tellurium-based HPONs.
研究不足
The study focuses on the synthesis and characterization of specific organic?inorganic hybrids, with potential limitations in the scalability and application of the synthesis methods.
1：Experimental Design and Method Selection:
The synthesis involved 'beaker chemistry' reaction of a mixture of K7H[Nb6O19]·13H2O and TeO2, followed by the addition of Cu(NO3)2·3H2O and organic amine. Blue crystals were formed by a di?usion method.
2：Sample Selection and Data Sources:
Samples were characterized by IR spectra, UV/vis, thermogravimetric analysis, and single crystal X-ray di?raction.
3：List of Experimental Equipment and Materials:
K7H[Nb6O19]·13H2O, TeO2, Cu(NO3)2·3H2O, organic amine.
4：Experimental Procedures and Operational Workflow:
The synthesis process involved mixing reagents, followed by diffusion method for crystal growth.
5：Data Analysis Methods:
Characterization techniques included IR spectra, UV/vis, thermogravimetric analysis, and single crystal X-ray di?raction.
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