研究目的
To analyze the diffraction time and the influence of strip moving speeds on texture measurement accuracy using an X-ray area detector, aiming to determine optimal parameters for online texture detection in steel production.
研究成果
A diffraction time of 2 s is optimal for balancing speed and accuracy in texture detection. Strip moving speeds up to 0.65 m/s have negligible influence on diffraction accuracy, enabling real-time online measurement. The XRD2 system, combined with fast texture detection theory, can be implemented in steel production for monitoring texture and mechanical properties.
研究不足
The study is conducted in a laboratory setting with an imitation online system, which may not fully replicate industrial conditions. The analysis is limited to IF steel and specific speed ranges (up to 0.65 m/s), and potential effects of higher speeds or other materials are not explored. Surface finish of specimens is assumed sufficient, but variations could affect results.
1:Experimental Design and Method Selection:
The study uses a laboratory two-dimensional X-ray diffraction (XRD2) system to analyze diffraction frames. The methodology involves determining diffraction time and assessing the effect of strip moving speeds on accuracy through absolute and relative error analyses.
2:Sample Selection and Data Sources:
Cold-rolled deep-drawing interstitial-free (IF) steel specimens with a thickness of
3:90 mm, taken from an industrial production line after continuous annealing, are used. Chemical compositions are provided in Table List of Experimental Equipment and Materials:
Equipment includes a V?NTEC-500 2D X-ray area detector, X-ray source, safety device, data collection and analysis device, proprietary goniometer, moving sample stage, and lead curtain for X-ray protection. Materials are IF steel specimens.
4:Experimental Procedures and Operational Workflow:
For diffraction time determination, diffraction frames are collected at times of
5:5, 1, 2, 3, 4, 5, 10, and 20 s using the area detector. For strip moving speed influence, specimens are moved at speeds of 1, 25, 45, and 65 m/s on the moving stage, with diffraction frames recorded at a fixed time of 2 s. Data is processed using γ-integration to analyze intensity counts. Data Analysis Methods:
Absolute and relative errors are calculated to evaluate accuracy. Statistical measures such as mean deviation (MD), range, and standard deviation (SD) are used for analysis, as detailed in Tables 2-5.
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