研究目的
To investigate the interfacial adhesion between embedded fibre optic sensors and epoxy matrix to find the best type of optical fibre to be used in epoxy matrices to produce smart composites.
研究成果
The ormoceramic-coated fibre with the smallest diameter (115 μm) exhibited the highest interfacial critical energy and least invasiveness, making it the best choice for smart composites in epoxy matrices. Polyacrylate fibres showed the poorest performance due to coating plasticity. Microscopy confirmed excellent adhesion of ormoceramic coatings to the matrix, with failures primarily at the cladding/coating interface. The study provides a basis for selecting optical fibres for structural health monitoring applications.
研究不足
The study did not apply surface treatments to the fibres, limiting analysis to inherent coating properties. The models assume perfect adhesion and may underestimate shear stress due to gradual failure processes. Sample fabrication was delicate due to fibre fragility, potentially introducing defects. The research focused on a specific epoxy matrix, and results may not generalize to other materials.
1:Experimental Design and Method Selection:
The study used pull-out tests to evaluate interfacial adhesion, adapted from micromechanical tests. Methods included optical microscopy and SEM analysis for interface characterization. Theoretical models from literature (e.g., Kelly et al., Nairn et al., Jiang et al.) were employed to calculate interfacial shear strength, maximum interfacial strength, and critical energy.
2:Sample Selection and Data Sources:
Four types of optical fibres with different coatings (polyimide, polyacrylate, ormoceramic) and diameters were used, supplied by FBGS Technologies, Germany. An epoxy resin E-227 (PROCHIMA, England) was used for the matrix. Samples were produced with specific embedded lengths.
3:List of Experimental Equipment and Materials:
Equipment included a mould for sample production, Instron 4302 testing machine with 1 kN load cell, optical microscope, Carl ZEISS EVO MA 10 SEM, JSM-7100F-JEOL SEM, sputter coater, and LOCTITE Hysol? 3425 adhesive. Materials included optical fibres, epoxy resin, alcohol for cleaning, and fibreglass tabs.
4:Experimental Procedures and Operational Workflow:
Fibres were cut to 90 mm, cleaned with alcohol, inserted into a mould with embedded lengths, resin was applied and cured at 80°C for 5 hours. Tabs were bonded to fibres for testing. Pull-out tests were conducted at 0.5 mm/min displacement rate using RTC method. Microscopy and SEM analyses were performed post-test to examine interfaces.
5:5 mm/min displacement rate using RTC method. Microscopy and SEM analyses were performed post-test to examine interfaces.
Data Analysis Methods:
5. Data Analysis Methods: Data from force-displacement curves were analyzed using equations for interfacial shear strength (τISS), maximum interfacial strength (τD), and critical energy (GC). Statistical methods were not specified, but averages were reported.
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