研究目的
To determine the phases of intermetallic compounds (IMCs) in SLID bonds, particularly for Cu-Sn and Au-Sn systems, to understand and predict bond properties such as thermal stability and material characteristics.
研究成果
Phase determination varies by SLID system: Cu-Sn phases are easily differentiated with microscopy and EDX, making routine analysis feasible, while Au-Sn phases require combined techniques like EBSD with EDX and microscopy for accurate identification due to complex phase diagrams and similar compositions. The study demonstrates the effectiveness of EBSD for spatial phase mapping in Au-Sn bonds.
研究不足
EDX has limited spatial resolution (~1 μm) and struggles with phases having similar stoichiometries; EBSD requires well-prepared, flat samples and is not as precise as X-ray diffraction; techniques may not be suitable for routine use in all laboratories due to equipment availability and sample preparation requirements.
1:Experimental Design and Method Selection:
The study focuses on comparing phase determination methods for Cu-Sn and Au-Sn SLID systems using microscopy, spectroscopy, and diffraction techniques.
2:Sample Selection and Data Sources:
Cu-Sn samples are prepared at wafer-level with electroplated Cu and Sn layers on Si substrates; Au-Sn samples are prepared at chip-level with electroplated Au layers and eutectic Au80Sn20 preforms on various substrates.
3:List of Experimental Equipment and Materials:
Equipment includes SEM, EDX, EBSD, optical microscope; materials include Cu, Sn, Au, Si substrates, Au80Sn20 preforms.
4:Experimental Procedures and Operational Workflow:
Bonding involves specific temperature profiles (e.g., 250-300°C for Cu-Sn, 300-350°C for Au-Sn) with holding times; characterization uses SEM with EDX and EBSD for phase analysis, and optical microscopy for contrast observation.
5:Data Analysis Methods:
EDX for compositional analysis, EBSD for crystallographic phase identification, and microscopy for visual differentiation.
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