研究目的
To investigate the effects of low-temperature tempering (210°C) on the microstructure, mechanical properties, and corrosion resistance of laser-cladded AISI 420 martensitic stainless steel coatings.
研究成果
Low-temperature tempering at 210°C refines the microstructure, increases ductility significantly with only a slight reduction in strength and hardness, and maintains comparable corrosion resistance to bulk AISI 420 SS, though with a slight decrease. This treatment provides a superior combination of mechanical properties and corrosion resistance for industrial applications.
研究不足
The study is limited to a specific tempering temperature (210°C) and time (1 hour); other temperatures or durations were not explored. The corrosion resistance showed a slight decrease after tempering, which may limit applications in highly corrosive environments. The research focuses on AISI 420 SS and may not be directly applicable to other materials.
1:Experimental Design and Method Selection:
The study involved laser cladding of AISI 420 SS powder onto an A36 steel substrate, followed by low-temperature tempering at 210°C for 1 hour. Microstructure and properties were analyzed using XRD, SEM, TEM, micro-hardness testing, tensile testing, and electrochemical polarization tests.
2:Sample Selection and Data Sources:
An A36 steel plate was used as the substrate, and spherical gas-atomized AISI 420 SS powder was supplied by Changsha Tianjiu Materials Ltd. Specimens were extracted from the laser-cladded coating before and after tempering.
3:List of Experimental Equipment and Materials:
Equipment included a TJ-HL-T5000 5 kW CO2 laser, Miniflex600 XRD, TM3030 SEM, JEOL-2100 TEM, HMV-2T micro-hardness tester, PWS-E100 universal testing machine, and CS300 electrochemical workstation. Materials included AISI 420 SS powder and A36 steel.
4:Experimental Procedures and Operational Workflow:
Laser cladding was performed with specific parameters (laser power
5:5 kW, scanning speed 6 mm/s, etc.), followed by tempering. Specimens were machined, polished, and characterized using various techniques. Tensile and corrosion tests were conducted according to standard methods. Data Analysis Methods:
Data were analyzed using techniques such as phase identification from XRD patterns, microstructural observation with SEM and TEM, hardness measurements, tensile property evaluation, and electrochemical parameter calculation from polarization curves.
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X-ray Diffractometer
Miniflex600
Rigaku Co.
Used for phase analysis of the specimens through X-ray diffraction.
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Scanning Electron Microscope
TM3030
Hitachi Ltd.
Used for microstructural characterization of the specimens.
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Transmission Electron Microscope
JEOL-2100
JEOL Ltd.
Used for detailed microstructural analysis and phase identification.
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Micro-hardness Tester
HMV-2T
Shimadzu Co.
Used to measure micro-hardness of the coatings.
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CO2 Laser
TJ-HL-T5000
Wuhan Unity Laser Co., Ltd.
Used for laser cladding process to deposit AISI 420 SS coating on the substrate.
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Universal Testing Machine
PWS-E100
Used for tensile testing of the specimens.
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Electrochemical Workstation
CS300
Wuhan Questt Asia Technology Co., Ltd.
Used for potentiodynamic polarization tests to evaluate corrosion resistance.
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Saturated Calomel Electrode
SCE
Used as reference electrode in electrochemical tests.
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Platinum Electrode
Used as counter electrode in electrochemical tests.
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CNC Mill
Used to machine off excess coating for specimen preparation.
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