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Studies on As-synthesized Graphene Oxide Flakes
摘要： Background: Due to the single atomic layer, flexible material, easily tuned of band gap, easily reduced to reduced graphene oxide, graphene oxide (GO) have a lot of application for Electronics, Biosensors, Biomedical application. Objective: The goal of the present work is to study the electrochemical properties of graphene oxide flakes. Method: In the present work, we synthesis of graphene oxide using modified hummer techniques. The morphological and structural characterization of as-prepared GO was investigated with the help of XRD, SEM, FTIR, UV, CV. Results: The XRD patterns of As-prepared graphene oxide (GO) flakes shows a peak at 11.2°, and the calculated value of lattice parameter comes out to be 15.56 A°. The peaks in the Raman spectrum are observed at 1599 cm-1 and 1349 cm-1, which confirms the lattice distortion in the graphene oxide (GO). The peaks in the FTIR spectrum of graphene oxide (GO) observed at, 3636 cm-1, 1753 cm-1, 1649 cm-1, 1456 cm-1, and 1177 cm-1 are attributed to O-H, C=O, C=C, C-OH, C-O bonds, respectively. The electrochemical studies of graphene oxide (GO) modified ITO electrode shows an improvement in the electrochemical parameters. Conclusion: We have prepared the graphene oxide by modified Hummers method. According to the electrochemical studies, graphene oxide (GO) modified ITO electrode is an excellent medium for the fast electron transfer between an electrode surface and electrolyte. On the basis of these studies, it is suggested that graphene oxide may be a best material for the fabrication of biosensors.
关键词： electrochemical studies,FTIR spectrum,Graphene oxide,raman spectrum,Biosensors,Biomedical application
更新于2025-09-19 17:15:36
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[IEEE 2019 IEEE International Conference on Electrical, Computer and Communication Technologies (ICECCT) - Coimbatore, India (2019.2.20-2019.2.22)] 2019 IEEE International Conference on Electrical, Computer and Communication Technologies (ICECCT) - Characterisation and performance evaluation of amorphous silicon nitride as passivation layer in thin film aSi:H solar cells
摘要： The fabrication and characterisation of amorphous silicon nitride layer is presented in this paper. The suitability of using it in photovoltaic application has been investigated. It is observed that the band gap of the nitride layers increases with increase in nitrogen content. The experimental results shows that amorphous silicon nitride alloy can be used as passivation layer in devices due to its high optical band gap. On the basis of experimental results, a thin ?lm aSi:H single junction solar cell having aSiNx as passivation layer has been proposed. Further, the behaviour of the proposed structure has been evaluated through simulation using SCAPS1D solar simulator. It is found out that the involvment of amorphous silicon nitride as passivation layer on the top part of the solar cell results in a conversion ef?ciency of 12.9 % and short circuit current density (Jsc) of 15.18 mA/cm2 which are signi?cant values as far as a single junction amorphous silicon thin ?lm solar cell has been considered. Furthermore, a comparison study on solar cell performance parameters of aSi:H solar cell with and without aSiNx passivation layer has been done.
关键词： composition pro?le,optical band gap,FTIR spectrum,passivation layer,PECVD,conversion ef?ciency
更新于2025-09-16 10:30:52
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Infrared Spectra for Alfa Fibers Treated with Thymol
摘要： In this work, we attempt to analyze the hydrogen bond network of cellulose by comparing the 2nd derivative infrared spectra of alfa fiber treated with different concentrations of thymol. It was proved, from this study, that the 2nd derivative infrared spectrum is a useful method for identifying the least changes incurred in the cellulosic supramolecular structure. It can be considered as an effective method to gain further insight on OH bond system of cellulosic materials and to clarify some grey areas in terms of infrared band assignment. The careful analysis of 2nd derivative infrared spectra of untreated and thymol treated alfa fibers revealed an increase in band intensity related to both intermolecular and intramolecular hydrogen bonds and a decrease in bands related to free hydroxyl groups.
关键词： Alfa fiber,FTIR spectrum,Cellulose,Hydrogen bonds,Thymol
更新于2025-09-10 09:29:36