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Spectral analysis and temperature measurement during flash sintering under AC electric field
摘要： In-situ diffraction experiments were used to study the change in peak profiles of 8YSZ during conventional sintering and flash sintering under AC electric field. Using calibration from a conventionally heated standard, the lattice expansion of 8YSZ under flash conditions was correlated to actual specimen temperature, indicating temperature comparable to that required for conventional sintering. At higher current densities, a temperature rise greater than 2000 °C was reached, which resulted in abnormal grain growth and temperature instability. Microstructural analysis demonstrated that finer grain size can be achieved by limiting the current in order to avoid high specimen temperatures. Experiments varying the thickness of the green compact resulted in higher heat loss due to thermal conduction and corresponding reduction in final density. A replacement to the blackbody radiation model was successfully used to fit the data and explain all effects based on Joule heating as well as provide a flash sintering processing map incorporating furnace temperature, power dissipation, and sample geometry.
关键词： 8YSZ,processing map,fast firing,flash sintering,energy dispersive diffraction
更新于2025-11-21 11:01:37
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Prediction of solidification cracking by an empirical-statistical analysis for laser cladding of Inconel 718 powder on a non-weldable substrate
摘要： This paper presents an empirical-statistical approach to predict solidification cracking during laser cladding of Inconel 718 powder on A-286 Fe-based superalloy. This approach is based on a linear regression analysis and empirical-statistical correlations between the key processing parameters (laser power, P; powder feed rate, F; and scanning speed, V) and the geometrical attributes of single laser cladding tracks. These correlations were used for the development of a processing map which assesses the effects of the geometrical characteristics on the solidification cracking and the required conditions to obtain crack-free clads. Scanning electron microscopy was used for microstructural characterization. Thermodynamic calculations using the non-equilibrium Scheil solidification model were also employed. The empirical-statistical analysis showed that the processing parameters directly associated with the height and angle of single laser cladding tracks are and, respectively. The processing map revealed that the dilution ratio is the governing macrostructural attribute required to avoid solidification cracking. Indeed, a substrate dilution ratio lower than 25% shifts the cladding composition to an alloy regime, which has lower susceptibility to solidification cracking. The role of this macrostructural feature in reducing the susceptibility of the fusion zone to solidification cracking is thoroughly discussed.
关键词： Thermodynamic simulation,Inconel 718,Processing map,Solidification cracking,Laser cladding,Dilution ratio
更新于2025-09-23 15:21:01