研究目的
To accurately measure the residual stresses in SLM-produced AlSi10Mg samples and understand its build-up mechanism during the SLM process by proposing a procedure coupling XRD with pretreatment consisting of mechanical polishing and chemical etching.
研究成果
The proposed procedure coupling XRD with pretreatment consisting of mechanical polishing and chemical etching effectively improves the accuracy and repetitiveness of residual stress measurements for SLM-produced AlSi10Mg samples by reducing the effect of surface roughness. Residual stresses are unevenly distributed on sample surfaces, with the major component along the building direction. The maximum residual stress approaches the yield strength of the material at room temperature where not released by cracks.
研究不足
The study focuses on SLM-produced AlSi10Mg samples, and the proposed procedure's effectiveness for other materials with high surface roughness needs further investigation. The total removed thickness of about 200 μm, though negligible compared to the sample height, might still affect the residual stress measurements.
1:Experimental Design and Method Selection:
The study involved the use of XRD technique coupled with pretreatment methods (mechanical polishing and chemical etching) to measure residual stresses in SLM-produced AlSi10Mg samples. The influence of surface roughness on residual stress measurements was investigated.
2:Sample Selection and Data Sources:
Commercial gas-atomized AlSi10Mg alloy powder was used for SLM samples. The samples were manufactured using a ProX DMP 200 SLM machine with specific process parameters.
3:List of Experimental Equipment and Materials:
ProX DMP 200 SLM machine, Zeiss Smartproof confocal microscope, PROTO iXRD-Portable X-ray diffractometer, SEM (TESCAN MAIA3), and various materials for sample preparation and surface treatment.
4:Experimental Procedures and Operational Workflow:
Samples were prepared using SLM, subjected to surface roughness measurement, residual stress measurement using XRD, and microstructure characterization. Surface treatment involved mechanical polishing and chemical etching.
5:Data Analysis Methods:
The slope of 2θ-sin2ψ straight line obtained from XRD measurements was used for calculating residual stresses. Surface roughness parameters were quantified using confocal microscopy.
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