研究目的
To explore the effects of laser parameters (power and scan speed) on the quality of an AISI H13 tool steel processed by an open-source AM machine, focusing on the processability of H13 tool steel by powder bed fusion and its microstructural characterization.
研究成果
The processing of AISI H13 tool steel in an open-parameter PBF machine was studied, revealing that microstructural features were mostly identical throughout the evaluated parameter window. The solidification structure was predominantly cellular, with C, Cr, and V segregation to the cell walls. The microstructure consisted of martensite and 16.5% to 29.7% retained austenite. A parameter set for minimal linear crack density, minimal porosity and maximum density was determined. Thermal diffusivity, thermal conductivity, and thermal capacity of as-built samples were measured, and the results were used to calculate dimensionless processing parameters.
研究不足
The study was limited to the evaluation of laser power and scan speed effects on the AISI H13 tool steel processed by powder bed fusion. Other parameters such as hatch spacing, layer thickness, or build plate temperature were not explored. The study also did not consider the microstructural changes caused by build plate temperature and how it may affect the consolidation of parts produced by AM.
1:Experimental Design and Method Selection:
Laser power (97-216 W) and scan speed (300-700 mm/s) were varied to evaluate the consolidation of parts, common defects, solidification structure, microstructure, and hardness.
2:Sample Selection and Data Sources:
Cubic samples of 10 × 10 × 10 mm were produced using a deposition strategy consisting of strokes with a maximum length of 5 mm and hatch spacing (h) of 80 μm.
3:List of Experimental Equipment and Materials:
AM OmniSint-160 machine equipped with Yb:YAG fiber laser, helium gas pycnometry, light optical microscopy (LOM), scanning electron microscopy (SEM), energy-dispersive x-ray spectroscopy (EDS), electron backscattered diffraction (EBSD), X-ray diffraction (XRD), Vickers hardness tester, nano hardness tester, laser flash analysis.
4:Experimental Procedures and Operational Workflow:
Samples were sectioned for metallography, mounted, ground, polished, and etched. Density and porosity were measured, and microstructural features were analyzed.
5:Data Analysis Methods:
Image processing for porosity estimation, XRD for phase determination, EBSD for grain orientation, hardness testing for mechanical properties.
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Coherent FieldMax II-To system
FieldMax II-To
Coherent
Laser power measurement
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Primes Focus Monitor FM 120
Focus Monitor FM 120
Primes
Laser beam spot size measurement
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Leica DMILM LED
DMILM LED
Leica
Light optical microscopy
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Thermo Fischer Quanta 650 FEG
Quanta 650 FEG
Thermo Fischer
Scanning electron microscopy
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Oxford Nordlys detector
Nordlys
Oxford
Electron backscattered diffraction analysis
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PANanalytical X’Pert PRO MRD XL diffractometer
X’Pert PRO MRD XL
PANanalytical
X-ray diffraction for phase determination
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Malvern Long Bench-MAM 5005 Mastersizer
Long Bench-MAM 5005 Mastersizer
Malvern
Powder size distribution measurement by laser diffraction
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AM OmniSint-160 machine
OmniSint-160
OmniTek
Powder bed fusion additive manufacturing
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Micromeritics AccuPyc 1330
AccuPyc 1330
Micromeritics
Helium gas pycnometry for density measurement
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Future Tech FV-800 tester
FV-800
Future Tech
Vickers hardness measurement
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CSM Instruments nano hardness tester
CSM Instruments
Nanoindentation experiments
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Netzsch LFA457 Microflash
LFA457 Microflash
Netzsch
Laser flash analysis for thermal diffusivity measurement
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