研究目的
To design and develop an instrument for in-situ temperature dependent diffuse reflectance spectroscopy (DRS) to explore the effect of temperature on optical properties of semiconducting materials.
研究成果
The in-house developed In-situ TD-DRS setup is capable of accurately characterizing the optical properties of semiconducting materials from room temperature to 500 K. It provides an economical alternative to existing designs without compromising data reliability. The setup is suitable for commercial applications and product development.
研究不足
The setup is limited to temperatures up to 500 K and optical spectral range of 200-800 nm.
1:Experimental Design and Method Selection:
The setup includes a heater, heating bath, temperature controller, DRS detector, UV-VIS spectrometer, and data analyzer.
2:Sample Selection and Data Sources:
Semiconducting oxides like BaTiO3 and TiO2 were used.
3:List of Experimental Equipment and Materials:
Includes a custom-designed heater, heating bath, CTC100 temperature controller, Agilent carry 60 UV-VIS spectrometer with DRS detector.
4:Experimental Procedures and Operational Workflow:
Samples were heated from room temperature to 500 K, and optical absorption spectra were recorded.
5:Data Analysis Methods:
Kubelka-Munk equation and Tauc equation were used for data analysis.
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