研究目的
Investigating the influence of heat treatment under hot isostatic pressing (HIP) on microstructure of intermetallic-reinforced tool steel manufactured by laser powder bed fusion.
研究成果
The study concluded that HIP influences phase transformations, necessitating a fundamental understanding of its impact on microstructure and the development of new post-processing regimes to ensure the best performance of the material.
研究不足
The study acknowledges that HIP influences phase transformations, indicating a need for a fundamental understanding of the influence of HIP on microstructure and the development of new post-processing regimes.
1:Experimental Design and Method Selection:
The study used a new approach where the whole cycle of the heat treatment was carried out in HIP under pressure. The microstructure of the steel was investigated by means of advanced microscopy and atom probe tomography.
2:Sample Selection and Data Sources:
A conventional steel grade of the same chemical composition, after a heat treatment at the same temperature-time conditions, was also characterized for comparison.
3:List of Experimental Equipment and Materials:
Stainless tool steel Uddeholm AM Corrax? powder was used to print the LPBF specimens. The specimens were produced using the EOS M290 system equipped with a 400 W fiber laser source.
4:Experimental Procedures and Operational Workflow:
The specimens were subjected to solution treatment and aging under pressure in HIP. The microstructure of the steel was investigated by means of advanced microscopy and atom probe tomography.
5:Data Analysis Methods:
The microstructure of the steel was analyzed using optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and atom probe tomography (APT).
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EOS M290 system
M290
EOS
Manufacturing LPBF specimens
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LECO V-100-C2 hardness tester
V-100-C2
LECO
Measuring Vickers hardness
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Leica DMI 3000 M
DMI 3000 M
Leica
Optical microscopy
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JEOL JEM 2100
JEM 2100
JEOL
Transmission electron microscopy
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Struers TenuPol-5
TenuPol-5
Struers
Electro-chemical preparation of TEM specimens
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URQ-HIP QIH48
QIH48
Quintus Technologies
HIP treatment
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LEO 1350 FEG SEM
1350 FEG
LEO
Scanning electron microscopy
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Seifert XRD 3003 PTS system
XRD 3003 PTS
Seifert
Phase analysis
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LEAP 3000X HR instrument
3000X HR
Imago Scientific Instruments
Atom probe tomography
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