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Preparation of high-porosity Al2O3 ceramic foams via selective laser sintering of Al2O3 poly-hollow microspheres

DOI:10.1016/j.ceramint.2019.10.144 期刊:Ceramics International 出版年份:2019 更新时间:2025-09-11 14:15:04
摘要: In this paper, high-porosity Al2O3 ceramic foams called Al2O3 PHM ceramics were fabricated through selective laser sintering (SLS) via Al2O3 poly-hollow microspheres (Al2O3 PHMs). SLS parameters were optimized by an orthogonal experiment as laser power = 6 W, scanning speed = 1800 mm/s, and scanning space = 0.15 mm. The effect of sintering temperature on microstructure, shrinkage, porosity, phase composition, mechanical properties and pore size distribution of Al2O3 PHM ceramics were investigated. When sintering temperature increased, Al2O3 PHM ceramics contained only Al2O3 phase and were gradually densified. With the raise of sintering temperature, the porosity of Al2O3 PHM ceramics decreased gradually from 77.09% to 72.41%, but shrinkage in H direction and compressive strength of Al2O3 PHM ceramics increased from 6.63% and 0.18 MPa to 13.10% and 0.72 MPa, respectively. Sintering temperature had little effect on pore size distribution of Al2O3 PHM ceramics, which only declined from 24.2 to 21.4 μm with the increase of sintering temperature from 1600 to 1650 °C. This method can not only directly prepare ceramic foams with complex shapes, but also control properties of ceramic foams. It provides a simple preparation method for many kinds of ceramic foams with complex structure and high porosity by using PHMs with different composition.
作者: Shan-Shan Liu,Meng Li,Jia-Min Wu,An-Nan Chen,Yu-Sheng Shi,Chen-Hui Li
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To fabricate high-porosity Al2O3 ceramic foams with complex shapes and controllable properties using selective laser sintering (SLS) of Al2O3 poly-hollow microspheres (Al2O3 PHMs).

Al2O3 PHM ceramic foams with complex structure and high porosity were successfully prepared by SLS using Al2O3 PHMs. The method allows for the control of ceramic foam properties and provides a simple preparation technique for various ceramic foams with complex structures and high porosity.

The compressive strength of the prepared Al2O3 PHM ceramic foams is not very high due to the fracture mode along the PHMs. The method might be improved by adding some sintering aids to enhance the strength of the sintering necks.

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