研究目的
To fabricate high-porosity Al2O3 ceramic foams with complex shapes and controllable properties using selective laser sintering (SLS) of Al2O3 poly-hollow microspheres (Al2O3 PHMs).
研究成果
Al2O3 PHM ceramic foams with complex structure and high porosity were successfully prepared by SLS using Al2O3 PHMs. The method allows for the control of ceramic foam properties and provides a simple preparation technique for various ceramic foams with complex structures and high porosity.
研究不足
The compressive strength of the prepared Al2O3 PHM ceramic foams is not very high due to the fracture mode along the PHMs. The method might be improved by adding some sintering aids to enhance the strength of the sintering necks.
1:Experimental Design and Method Selection:
The study optimized SLS parameters (laser power, scanning speed, scanning space) through an orthogonal experiment to prepare Al2O3 PHM ceramics.
2:Sample Selection and Data Sources:
Al2O3 PHMs were calcined and mixed with epoxy resin E12 as a sacrificial binder.
3:List of Experimental Equipment and Materials:
SLS machine (C250, Wuhan Huake 3D Technology Co., Ltd., China), Al2O3 PHMs, epoxy resin E
4:Experimental Procedures and Operational Workflow:
Green bodies were formed via SLS, then de-binded and sintered at various temperatures to study the effect on microstructure, porosity, and mechanical properties.
5:Data Analysis Methods:
Properties of the ceramics were analyzed using SEM, XRD, TG/DTA, and mechanical testing.
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