研究目的
Investigating the effect of Ti addition on the wetting and brazing of Sn0.3Ag0.7Cu filler on SiC ceramic.
研究成果
The addition of Ti significantly enhanced the wetting and spreading behavior of SAC-Ti on the SiC. The lowest equilibrium contact angle of 9° was obtained with 1.5 wt.% Ti content filler. The wetting of SAC-Ti on SiC was reaction-controlled. Completely filled SiC/SiC joints were obtained with the Ti content in filler higher than 0.5 wt.%. The highest joints shear strength of 35.7 MPa was obtained with SAC-1.5 wt.% Ti filler.
研究不足
The study is limited to the effect of Ti addition on the wetting and brazing of Sn0.3Ag0.7Cu filler on SiC ceramic. The experiments were conducted under specific conditions (1223 K for 10 minutes). The study does not explore the effect of other active elements or different brazing conditions.
1:Experimental Design and Method Selection:
The wetting behavior was investigated using the sessile drop method. SiC/SiC was brazed by SAC-Ti filler with different Ti content at 1223 K (950 °C) for 10 minutes.
2:Sample Selection and Data Sources:
Sintered SiC and SAC-Ti fillers were used. The SiC bulks were mechanically ground and polished, then ultrasonically cleaned.
3:List of Experimental Equipment and Materials:
SEM (Merlin Compact, Zeiss), EDX (Octane Plus, EDAX), XRD (DX-2700), TEM (JEOL-2100), universal testing machine (Instron 5967).
4:7).
Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: The sessile drop experiments were conducted under a vacuum. The metal cylinder was placed on the top of SiC and heated to testing temperature. The profiles of the molten metal droplet were photographed by a Nikon camera.
5:Data Analysis Methods:
The contact angles were analyzed by an axisymmetric drop shape analysis program. The microstructure and element distribution were investigated by SEM and EDX. The reaction phases were identified by XRD and TEM.
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